S-甲基 4-甲基苯硫代磺酸酯合成路线 （共 24 条）
反应条件
sodium hydrogencarbonate; sodium chloride; molecular sieve in N-methyl-acetamide
参考文献
L'Oreal
Patent: US5296611 A1, 1994 ;
反应条件
sodium periodate in water
T=20°C; 0.5 h;
参考文献
Takata, Toshikazu; Kim, Yong Hae; Oae, Shigeru
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 5 p. 1443 - 1447
反应条件
in water; acetone
T=50°C; 2 h; Title compound not separated from byproducts.;
参考文献
Duffy, Stephen; Langler, Richard F.
Australian Journal of Chemistry, 2008 , vol. 61, # 6 p. 466 - 471
反应条件
1: 92 percent / sulfur / pyridine / 48 h / Ambient temperature
2: 1.) Amberlyst A-26 (Cl(1-) form) / 1.) H2O, r.t., 18 h; 2.) benzene, reflux, 19 h
View Scheme
参考文献
Takano, Seiichi; Hiroya, Kou; Ogasawara, Kunio
Chemistry Letters, 1983 , p. 255 - 256
反应条件
in water; benzene
T=50°C; 24 h; Title compound not separated from byproducts.;
参考文献
Duffy, Stephen; Langler, Richard F.
Australian Journal of Chemistry, 2008 , vol. 61, # 6 p. 466 - 471
反应条件
in water; acetone
Heating;
参考文献
Weidner,J.P.; Block,S.S.
J. Med. Chem., 1964 , vol. 7, p. 671 - 673
参考文献
Autrey,R.L.; Scullard,P.W.
Journal of the American Chemical Society, 1968 , vol. 90, p. 4924 - 4929
参考文献
Harpp,D.N. et al.
Journal of Organic Chemistry, 1979 , vol. 44, # 23 p. 4135 - 4140
反应条件
1: 95 percent / CCl4 / 50 - 60 °C
2: 1) ether, 18 deg C; 2) reflux
View Scheme
参考文献
Senning, Alexander; Hansen, Holger C.; Abdel-Megeed, Mohamed F.; Mazurkiewicz, Witold; Jensen, Birgit
Tetrahedron, 1986 , vol. 42, # 2 p. 739 - 746
反应条件
Amberlyst A-26 (Cl(1-) form)
1.) H2O, r.t., 18 h; 2.) benzene, reflux, 19 h; Yield given. Multistep reaction;
参考文献
Takano, Seiichi; Hiroya, Kou; Ogasawara, Kunio
Chemistry Letters, 1983 , p. 255 - 256
