4,5-双(甲硫代)-1,3-二硫杂环戊烯-2-硫酮合成路线 （共 25 条）
反应条件
triethyl phosphite T=120 - 130°C; 0.666667 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 9 p. 2563 - 2565
反应条件
1: P(OEt)3 / benzene / 19.5 h / Heating 2: 65 percent / LiBr / hexamethylphosphoric acid triamide / 0.37 h / 145 - 147 °C View Scheme
参考文献
Papavassiliou, G.C.; Zambounis, J.S.; Mousdis, G.A.; Gionis, V.; Yiannopoulos, S.Y.
Molecular Crystals and Liquid Crystals (1969-1991), 1988 , vol. 156, p. 269 - 276
反应条件
tetra-(n-butyl)ammonium iodide
1.) DMF, electrochemical reduction: mercury pool, 2.) 0.5 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Falsig, Mogens; Lund, Henning
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1980 , vol. 34, # 8 p. 591 - 596
反应条件
triethyl phosphite in toluene
T=120°C; 3 h;
参考文献
Jia, Chunyang; Liu, Shi-Xia; Neels, Antonia; Stoeckli-Evans, Helen; Decurtins, Silvio
Synthesis, 2005 , # 13 art. no. T16004SS, p. 2157 - 2160
反应条件
mercury(II) diacetate in chloroform; acetic acid
5 h; Heating;
参考文献
Hartke, Klaus; Kissel, Thomas; Quante, Josef; Matusch, Rudolf
Chemische Berichte, 1980 , vol. 113, # 5 p. 1898 - 1906
