N,N’-二(对甲苯磺酰基)-1,2-苯二胺合成路线 (共 14 条)
反应条件
1: 4 N aq. sodium hydroxide / 0.33 h / Heating 2: conc. sulphuric acid / 4 h / Heating 3: 70 percent / glacial acetic acid / methanol / 0.5 h / Ambient temperature View Scheme
参考文献
Reddy, A. Pandu Ranga; Veeranagaiah, V.; Ratnam, C. V.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 367 - 371
反应条件
1: 80 percent / Br2 in AcOH, NaOAc 2: 90 percent / sulphuric acid View Scheme
参考文献
Wasik, Romualda; Winska, Patrycja; Poznanski, Jaroslaw; Shugar, David
Journal of Physical Chemistry B, 2012 , vol. 116, # 24 p. 7259 - 7268
反应条件
1: pyridine 2: sodium methylate; methanol / und Erwaermen des Reaktionsloesung mit CH3I 3: aqueous H2SO4 View Scheme
参考文献
Cheesman
Journal of the Chemical Society, 1955 , p. 3308
反应条件
1: 89 percent / Br2, acetic acid, sodium acetate 2: 83.5 percent / sulfuric acid 3: 76 percent / thionyl chloride, pyridine / 3 h / Heating View Scheme
参考文献
Shao, Jinjun; Chang, Jingjing; Chi, Chunyan
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 35 p. 7045 - 7052
反应条件
perchloric acid; acetic acid 1 h; Heating;
参考文献
Kudav, D.P.; Samant,S.P.; Hosangadi, B.D.
Synthetic Communications, 1987 , vol. 17, # 10 p. 1185 - 1188
反应条件
1: 4 N aq. sodium hydroxide / 0.33 h / Heating 2: conc. sulphuric acid / 4 h / Heating View Scheme
参考文献
Reddy, A. Pandu Ranga; Veeranagaiah, V.; Ratnam, C. V.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 367 - 371
反应条件
1: 4 N aq. sodium hydroxide / 0.33 h / Heating 2: conc. sulphuric acid / 4 h / Heating View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 24, p. 367 - 371
反应条件
pyridine in dichloromethane
3 h; Ambient temperature;
参考文献
Avdeenko
Russian Journal of Organic Chemistry, 1998 , vol. 34, # 4 p. 515 - 524
参考文献
Dubey; Kulkarni, Subhash M.; Vinod Kumar
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2002 , vol. 41, # 6 p. 1305 - 1309
参考文献
Bhosale, Sheshanath V.; Bhosale, Sidhanath V.; Kalyankar, Mohan B.; Langford, Steven J.
Organic Letters, 2009 , vol. 11, # 23 p. 5418 - 5421