2,4,6-三异丙基苯甲酸合成路线 （共 21 条）
反应条件
sodium hydride in tetrahydrofuran 19 h; Ambient temperature;
参考文献
Beak, Peter; Becker, Peter D.
Journal of Organic Chemistry, 1982 , vol. 47, # 20 p. 3855 - 3861
反应条件
diethyl ether; phenyllithium anschliessend Behandeln mit CO2;
参考文献
Fuson; Horning
Journal of the American Chemical Society, 1940 , vol. 62, p. 2962
反应条件
1: tetrachloromethane; iron; bromine / 0 °C / Lichtausschluss 2: magnesium; diethyl ether / Behandeln der Reaktionsloesung mit festem Kohlendioxid View Scheme
参考文献
Fuson; Horning
Journal of the American Chemical Society, 1940 , vol. 62, p. 2962
反应条件
NOBF4 in acetonitrile
参考文献
Olah,G.A.; Olah,J.A.
Journal of Organic Chemistry, 1965 , vol. 30, p. 2386 - 2387
反应条件
1: NaH / 40 h / Heating 2: 1.) sec-BuLi, TMEDA / 1.) THF, -98 deg C, 2.) a) -98 deg C, b) from -98 deg C to RT 3: 90 percent / NaH / tetrahydrofuran / 19 h / Ambient temperature View Scheme
参考文献
Beak, Peter; Becker, Peter D.
Journal of Organic Chemistry, 1982 , vol. 47, # 20 p. 3855 - 3861
反应条件
1: 1.) sec-BuLi, TMEDA / 1.) THF, -98 deg C, 2.) a) -98 deg C, b) from -98 deg C to RT 2: 90 percent / NaH / tetrahydrofuran / 19 h / Ambient temperature View Scheme
参考文献
Beak, Peter; Becker, Peter D.
Journal of Organic Chemistry, 1982 , vol. 47, # 20 p. 3855 - 3861
反应条件
(i) tBuLi, THF, hexane, (ii) /BRN= 1900390/; Multistep reaction;
参考文献
Beak, Peter; Carter, Linda G.
Journal of Organic Chemistry, 1981 , vol. 46, # 11 p. 2363 - 2373
参考文献
Wagner, Peter J.; Meador, Michael A.; Zhou, Boli; Park, Bong-Ser
Journal of the American Chemical Society, 1991 , vol. 113, # 25 p. 9630 - 9639
参考文献
Fuson; Horning
Journal of the American Chemical Society, 1940 , vol. 62, p. 2962
参考文献
Fuson; Denton; Best
Journal of Organic Chemistry, 1943 , vol. 8, p. 64,69
