1,3-二氢-2H-吲哚-2-硫酮合成路线 （共 17 条）
反应条件
tetraphosphorus decasulfide; sodium hydrogencarbonate in tetrahydrofuran T=20°C; 4 h;
参考文献
VIRONOVA AB; PETTERSSON, Birgitta; HASIMBEGOVIC, Vedran; SVENSSON, Per, H.; BERGMAN, Jan
Patent: WO2012/104415 A1, 2012 ;
Location in patent: Page/Page column 10 ;
反应条件
sodium hydrogencarbonate in tetrahydrofuran; benzene
参考文献
Shionogi and Co., Ltd.
Patent: US4256640 A1, 1981 ;
反应条件
1: With sodium tetrahydroborate in tetrahydrofuran T=40 - 45°C; 3 h; Inert atmosphere; 2: With water in tetrahydrofuran 24 h;
参考文献
VIRONOVA AB; PETTERSSON, Birgitta; HASIMBEGOVIC, Vedran; SVENSSON, Per, H.; BERGMAN, Jan
Patent: WO2012/104415 A1, 2012 ;
Location in patent: Page/Page column 9; 10 ;
参考文献
McNeil Laboratories, Incorporated
Patent: US4059583 A1, 1977 ;
反应条件
1: 55 percent / hydrazine hydrate / 4 h / 140 °C 2: 83 percent / P2S5; Na2CO3 / tetrahydrofuran / 0 - 20 °C View Scheme
参考文献
Thanigaimalai, Pillaiyar; Lee, Ki-Cheul; Sharma, Vinay Kumar; Sharma, Niti; Roh, Eunmiri; Kim, Youngsoo; Jung, Sang-Hun
Chemical and Pharmaceutical Bulletin, 2011 , vol. 59, # 10 p. 1285 - 1288
反应条件
1: 45 percent / AlCl3, NaCl / 1.) 140 deg C, 2.) 220 deg C, 5 min 2: 49 percent / P2S5 / dioxane / 0.5 h / Heating View Scheme
参考文献
Sugasawa et al.
Yakugaku Zasshi, 1938 , vol. 58, p. 139;engl.Ref.S.29
Chem.Abstr., 1938 , p. 4161
反应条件
in benzene 0.5 h; Heating;
参考文献
Baudin, Jean-Bernard; Julia, Sylvestre A.; Lorne, Robert
Bulletin de la Societe Chimique de France, 1987 , # 1 p. 181 - 188
参考文献
Rewcastle, Gordon W; Janosik, Tomasz; Bergman, Jan
Tetrahedron, 2001 , vol. 57, # 33 p. 7185 - 7189
反应条件
sulfuric acid Electrolysis.Verwendung einer Blei-Kathode;
参考文献
Sugasawa et al.
Yakugaku Zasshi, 1938 , vol. 58, p. 139;engl.Ref.S.29
Chem.Abstr., 1938 , p. 4161
反应条件
ammonium cerium(IV) nitrate; silica gel in acetonitrile T=60°C; 5.5 h;
参考文献
Banerjee, Satarupa; Sarkar, Sandipan; Basak, Ramkrishna; Chakrabarty, Manas
Journal of the Indian Chemical Society, 2004 , vol. 81, # 2 p. 169 - 170
