1,3-二氢异苯并呋喃合成路线 （共 101 条）
反应条件
1: With 2-hydroxy-1,3-isoindolinedione; 2,2'-azo-bisisobutyronitrile; oxygen in acetonitrile T=75°C; P=760.051 Torr; 20 h; 2: With triphenylphosphine in acetonitrile T=25°C; Further stages.;
参考文献
Advanced Synthesis and Catalysis, , vol. 343, # 8 p. 809 - 813
反应条件
naphthalene; lithium 1.) THF, 0 deg C, 2 h, 2.) THF, -10 deg C, 60 min; Yield given. Multistep reaction;
参考文献
Azzena, Ugo; Demartis, Salvatore; Melloni, Giovanni
Journal of Organic Chemistry, 1996 , vol. 61, # 15 p. 4913 - 4919
反应条件
1: 1) sec-BuLi / 1) THF, -40 deg C, 2 h, 2) THF, 1 h 2: 1) Li, naphthalene, 2) H2O / 1) THF, 0 deg C, 3 h View Scheme
参考文献
Azzena, Ugo; Demartis, Salvatore; Melloni, Giovanni
Journal of Organic Chemistry, 1996 , vol. 61, # 15 p. 4913 - 4919
反应条件
dihydrogen peroxide; trifluoroacetic acid; zinc dibromide in 1,4-dioxane; water T=100°C; 16 h;
参考文献
Tetrahedron Letters, , vol. 53, # 45 p. 6123 - 6126
反应条件
1: With 2-hydroxy-1,3-isoindolinedione; 2,2'-azo-bisisobutyronitrile; oxygen in acetonitrile T=75°C; P=760.051 Torr; 20 h; 2: With triphenylphosphine in acetonitrile T=25°C; Further stages.;
参考文献
Advanced Synthesis and Catalysis, , vol. 343, # 8 p. 809 - 813
反应条件
nitric acid; acetic acid in water T=60 - 80°C; 0.5 - 4 h; Product distribution / selectivity;
参考文献
EP1350785 A1, ;
Page/Page column 3-4 ;
反应条件
nitric acid; acetic acid in water T=70°C; 1 h; Product distribution / selectivity;
参考文献
EP1350785 A1, ;
Page/Page column 4 ;
反应条件
oxygen; sodium hydroxide in toluene T=89.84°C; P=3750.38 Torr; 1 h; Autoclave;
参考文献
Applied Catalysis A: General, , vol. 394, # 1-2 p. 79 - 85
