1,3-二氢异苯并呋喃合成路线 （共 101 条）
反应条件
caesium carbonate; Pd[P(t-Bu3)]2 in 1,4-dioxane; water T=20 - 100°C;
参考文献
EP2062901 A1, ;
Page/Page column 13 ;
反应条件
sodium methylate in carbonic acid dimethyl ester; acetonitrile 4 h; Inert atmosphere;
参考文献
ChemSusChem, , vol. 5, # 8 p. 1578 - 1586
反应条件
aluminum oxide 0.1 h; microwave irradiation;
参考文献
Synlett, , # 9 p. 1526 - 1528
反应条件
sodium hydroxide in water T=100°C; pH=12; 4 h;
参考文献
US6372921 B1, ;
Example 33 ;
反应条件
sodium hydroxide in water T=100°C; pH=7; 4 h;
参考文献
US6372921 B1, ;
Example 16 ;
反应条件
hydrogenchloride in water T=70°C; 1 h;
参考文献
US6372921 B1, ;
Example 18 ;
反应条件
1: 74 percent / PCC / CH2Cl2 / 1.5 h / Ambient temperature 2: 91 percent / ethanol / 1.) 60 deg C, 3 h, 2.) room temp., 3 h, 3.) -20 deg C, overnight 3: 0.2 M NaOC2H5 / ethanol / 2 h / Ambient temperature; Irradiation View Scheme
参考文献
Journal of the American Chemical Society, , vol. 111, # 4 p. 1465 - 1473
反应条件
1: 91 percent / ethanol / 1.) 60 deg C, 3 h, 2.) room temp., 3 h, 3.) -20 deg C, overnight 2: 0.2 M NaOC2H5 / ethanol / 2 h / Ambient temperature; Irradiation View Scheme
参考文献
Journal of the American Chemical Society, , vol. 111, # 4 p. 1465 - 1473
反应条件
1: 63 percent / PCC 2: 79 percent / 1.) 60 deg C, 3 h, 2.) room temp., 3 h, 3.) -20 deg C, overnight 3: 0.2 M NaOCH3 / methanol / 2 h / Ambient temperature; Irradiation View Scheme
参考文献
Journal of the American Chemical Society, , vol. 111, # 4 p. 1465 - 1473
反应条件
1: 79 percent / 1.) 60 deg C, 3 h, 2.) room temp., 3 h, 3.) -20 deg C, overnight 2: 0.2 M NaOCH3 / methanol / 2 h / Ambient temperature; Irradiation View Scheme
参考文献
Journal of the American Chemical Society, , vol. 111, # 4 p. 1465 - 1473
