N-苄氧甲酰甘氨酸硫代酰胺合成路线 （共 5 条）
反应条件
Lawesson's reagent in tetrahydrofuran T=25°C; 4 h;
参考文献
Koerber-Ple; Massiot
Journal of Heterocyclic Chemistry, 1995 , vol. 32, # 4 p. 1309 - 1315
反应条件
Dowex 1X8 SH(1-); hydrogen sulfide in methanol T=20°C; 3 h;
参考文献
Liboska, Radek; Zyka, Daniel; Bobek, Miroslav
Synthesis, 2002 , # 12 p. 1649 - 1651
反应条件
1: 91 percent / KHCO3 / H2O; dioxane / 2 h 2: 95 percent / Lawesson's reagent / tetrahydrofuran / 4 h / 25 °C View Scheme
参考文献
Clausen, Kim; Thorsen, Michael; Lawesson, Sven-Olov; Spatola, Arno F.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 4 p. 785 - 798
反应条件
hydrogen sulfide; potassium carbonate 1.) Et2O, 0.5 h, 2.) Et2O, 0 deg C, 1 h; Yield given. Multistep reaction;
参考文献
Clausen, Kim; Thorsen, Michael; Lawesson, Sven-Olov; Spatola, Arno F.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 4 p. 785 - 798
反应条件
hydrogen bromide in ethyl acetate
参考文献
Journal of the American Chemical Society, , vol. 95, p. 5677 - 5679
