1-苯基-2-丁烯-1-酮合成路线 (共 117 条)
反应条件
tris-(dibenzylideneacetone)dipalladium(0); tris(4-methylphenyl)-phosphine in toluene T=100°C; 12 h; Inert atmosphere;
参考文献
Rodriguez, Nuria; Manjolinho, Filipe; Gruenberg, Matthias F.; Goossen, Lukas J.
Chemistry - A European Journal, 2011 , vol. 17, # 49 p. 13688 - 13691
反应条件
boron trifluoride diethyl etherate; mercury(II) diacetate in acetic acid Ambient temperature;
参考文献
Liotta, Dennis; Zima, George
Journal of Organic Chemistry, 1980 , vol. 45, # 12 p. 2551 - 2553
反应条件
benzoylchlorobis(triphenylphosphine)palladium(II) in chloroform T=65°C; 4.5 h;
参考文献
Labadie, Jeff W.; Tueting, David; Stille, J. K.
Journal of Organic Chemistry, 1983 , vol. 48, # 24 p. 4634 - 4642
反应条件
amberlyst-15 in dichloromethane T=25°C; 1 h;
参考文献
Tivola, Paolo Balma; Deagostino, Anna; Prandi, Cristina; Venturello, Paolo
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 4 p. 437 - 441
反应条件
palladium (II) trifluoroacetate in tetrahydrofuran T=70°C;
参考文献
Obora, Yasushi; Nakanishi, Masafumi; Tokunaga, Makoto; Tsuji, Yasushi
Journal of Organic Chemistry, 2002 , vol. 67, # 16 p. 5835 - 5837
反应条件
1: (2-Oxo-2-phenylethyl)triphenylphosphonium bromide With sodium hydroxide in dichloromethane 2: acetaldehyde Wittig reaction; 1 h; Further stages.;
参考文献
Therkelsen, Frans D.; Hansen, Anne-Lene L.; Pedersen, Erik B.; Nielsen, Claus
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 16 p. 2908 - 2918
反应条件
nickel in ethylene glycol dimethyl ether T=85°C; 0.5 h;
参考文献
Inaba, Shin-ichi; Rieke, Reuben D.
Journal of Organic Chemistry, 1985 , vol. 50, # 9 p. 1373 - 1381
反应条件
tris-(dibenzylideneacetone)dipalladium(0); potassium carbonate; tris(4-methylphenyl)-phosphine in 1,3,5-trimethyl-benzene T=150°C; 12 h; Inert atmosphereMolecular sieve;
参考文献
Rodriguez, Nuria; Manjolinho, Filipe; Gruenberg, Matthias F.; Goossen, Lukas J.
Chemistry - A European Journal, 2011 , vol. 17, # 49 p. 13688 - 13691
反应条件
chromium(VI) oxide in diethyl ether; water
参考文献
Provencher, Brian A.; Bartelson, Keith J.; Liu, Yan; Foxman, Bruce M.; Deng, Li
Angewandte Chemie - International Edition, 2011 , vol. 50, # 45 p. 10565 - 10569
反应条件
vanadium(III) chloride 1.) dichloromethane, -78 deg C, 2 h; 2.) toluene, reflux, 16 h;
参考文献
Hirao, Toshikazu; Misu, Daisuke; Agawa, Toshio
Journal of the American Chemical Society, 1985 , vol. 107, # 24 p. 7179 - 7181