1-甲基-1-苯基-3-苯甲酰基硫脲合成路线 （共 8 条）
反应条件
hydrazine T=25°C; 0.166667 h;
参考文献
Kodomari, Mitsuo; Suzuki, Masato; Tanigawa, Keiko; Aoyama, Tadashi
Tetrahedron Letters, 2005 , vol. 46, # 35 p. 5841 - 5843
反应条件
in methanol T=25°C; 4-bromophenolate buffer; Rate constant;
参考文献
Kavalek, Jaromir; Jirman, Josef; Sterba, Vojeslav
Collection of Czechoslovak Chemical Communications, 1985 , vol. 50, # 3 p. 766 - 778
反应条件
1: benzoyl chloride With potassium thioacyanate in acetone
T=50°C; 0.75 h;
2: N-methylaniline in acetone
T=35°C; 1.5 h;
参考文献
Mandal, Haridas; Ray, Debashis
Inorganica Chimica Acta, 2014 , vol. 414, p. 127 - 133
反应条件
in acetone
Addition; 0.5 h; reflux;
参考文献
Shanmuga Sundara Raj; Puviarasan; Velmurugan; Jayanthi; Fun, Hoong-Kun
Acta Crystallographica Section C: Crystal Structure Communications, 1999 , vol. 55, # 8 p. 1318 - 1320
反应条件
1: sodium isothiocyanate; benzoyl chloride in acetone
T=0°C; Substitution;
2: N-methylaniline in acetone
T=20°C; Addition;
参考文献
Chan, Chung Woo; Ng, Chun Ming Dominic; Ho, Joyce; Tin, Kam Chung
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 1997 , vol. 36, # 3 p. 216 - 219
反应条件
1: ammonium thiocyanate
2: acetone / 4 h
View Scheme
参考文献
Tan, Siew San; Al-Abbasi, Aisha A.; Mohamed Tahir, Mohamed Ibrahim; Kassim, Mohammad B.
Polyhedron, 2014 , vol. 68, p. 287 - 294
反应条件
1.) Me2CO, 40 deg C, 30 min, 2.) Me2CO, 20 deg C, 2 h; Yield given. Multistep reaction;
参考文献
Brindley, Jocelyn C.; Caldwell, Jennifer M.; Meakins, G. Denis; Plackett, Simon J.; Price, Susan J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1153 - 1158
反应条件
triethylamine in ethanol
2 h; Heating;
参考文献
Brindley, Jocelyn C.; Caldwell, Jennifer M.; Meakins, G. Denis; Plackett, Simon J.; Price, Susan J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1153 - 1158
