2,3-二氢-1H-苯并[e]茚合成路线 （共 41 条）
反应条件
platinum (II) chloride in toluene
T=100°C; Bergman reaction; 10 h;
参考文献
Taduri, Bhanu Pratap; Ran, Ying-Fen; Huang, Chun-Wei; Liu, Rai-Shung
Organic Letters, 2006 , vol. 8, # 5 p. 883 - 886
反应条件
dirhodium tetraacetate; lithium tert-butylate in toluene
T=90°C; 1 h; Inert atmosphereMolecular sieve;
参考文献
Xia, Ying; Liu, Zhenxing; Xiao, Qing; Qu, Peiyuan; Ge, Rui; Zhang, Yan; Wang, Jianbo
Angewandte Chemie - International Edition, 2012 , vol. 51, # 23 p. 5714 - 5717
反应条件
P2O5 in benzene
Heating;
参考文献
Lee-Ruff, Edward; Hopkinson, Alan C.; Kazarians-Moghaddam, Hira; Duperrouzel, Paul; Gupta, Brij; Katz, Morris
Tetrahedron Letters, 1981 , vol. 22, # 49 p. 4917 - 4920
反应条件
potassium hydroxide; hydrazine hydrate; Trimethylene glycol
T=195°C;
参考文献
Muneyuki,R.; Tanida,H.
Journal of the American Chemical Society, 1968 , vol. 90, p. 656 - 662
参考文献
Beloglazkina, Elena K.; Majouga, Alexander G.; Mironov, Andrei V.; Yudina, Anna V.; Moiseeva, Anna A.; Lebedeva, Maria A.; Khlobystov, Andrei N.; Zyk, Nikolai V.
Polyhedron, 2013 , vol. 63, p. 15 - 20
反应条件
potassium hydroxide; hydrazine hydrate; diethylene glycol
参考文献
Cope et al.
Journal of the American Chemical Society, 1956 , vol. 78, p. 2551,2555
反应条件
palladium on activated charcoal
T=250 - 350°C;
参考文献
Gutsche,C.D.; Bowers,J.E.
Journal of Organic Chemistry, 1967 , vol. 32, p. 1203 - 1212
反应条件
2: NO2, NaOAc
3: NaOEt
4: (reduction)
5: Pd-C / 250 - 350 °C
View Scheme
参考文献
Gutsche,C.D.; Bowers,J.E.
Journal of Organic Chemistry, 1967 , vol. 32, p. 1203 - 1212
反应条件
1: NO2, NaOAc
2: NaOEt
3: (reduction)
4: Pd-C / 250 - 350 °C
View Scheme
参考文献
Gutsche,C.D.; Bowers,J.E.
Journal of Organic Chemistry, 1967 , vol. 32, p. 1203 - 1212
反应条件
1: (i) pyrrolidine, (ii) /BRN= 605310/
3: NO2, NaOAc
4: NaOEt
5: (reduction)
6: Pd-C / 250 - 350 °C
View Scheme
参考文献
Gutsche,C.D.; Bowers,J.E.
Journal of Organic Chemistry, 1967 , vol. 32, p. 1203 - 1212
