2-氨基-4-甲基二苯甲酮合成路线 (共 17 条)
反应条件
zinc T=70 - 72°C; Friedel-Crafts acylation; 0.00277778 h; microwave irradiation;
参考文献
Synthesis, , # 18 p. 2877 - 2881
反应条件
aluminium trichloride; boron trichloride in dichloromethane; xylene T=120°C; Friedel-Crafts reaction;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 12, # 2 p. 249 - 253
反应条件
1: With silver hexafluoroantimonate; {RuCl2(1-methyl-4-(1-methylethyl)benzene)}2; copper (II) acetate monohydrate in 1,2-dichloro-ethane T=100°C; 24 h; Inert atmosphereSchlenk technique; 2: With sulfuric acid T=0 - 20°C; 2 h; Inert atmosphereSchlenk technique; 3: With sodium hydrogencarbonate Inert atmosphereSchlenk technique;
参考文献
Chemical Communications, , vol. 49, # 45 p. 5225 - 5227
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 2940 - 2948
反应条件
1.1: 87 percent / iron; acetic acid / ethanol 2.1: tetrahydrofuran 2.2: ammonium chloride / H2O 2.3: hydrochloric acid / methanol View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 2, , # 2 p. 214 - 228
反应条件
1.1: 70 percent 2.1: 87 percent / iron; acetic acid / ethanol 3.1: tetrahydrofuran 3.2: ammonium chloride / H2O 3.3: hydrochloric acid / methanol View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 2, , # 2 p. 214 - 228
反应条件
1: potassium acetate 2: chromium (VI)-oxide; acetic acid / und Erwaermen des Reaktionsprodukts mit aethanol.Kalilauge View Scheme
参考文献
Journal and Proceedings of the Royal Society of New South Wales, , vol. 80, p. 33,40
反应条件
1: concentrated aqueous hydrochloric acid 2: potassium acetate 3: chromium (VI)-oxide; acetic acid / und Erwaermen des Reaktionsprodukts mit aethanol.Kalilauge View Scheme
参考文献
Journal and Proceedings of the Royal Society of New South Wales, , vol. 80, p. 33,40
反应条件
1: concentrated aqueous hydrochloric acid 2: potassium acetate 3: chromium (VI)-oxide; acetic acid / und Erwaermen des Reaktionsprodukts mit aethanol.Kalilauge View Scheme
参考文献
Journal and Proceedings of the Royal Society of New South Wales, , vol. 80, p. 33,40
反应条件
chromium(VI) oxide; acetic acid Erhitzen des Reaktionsprodukts mit wss. Schwefelsaeure;
参考文献
Journal and Proceedings of the Royal Society of New South Wales, , vol. 80, p. 33,40