螺[环己烷-1,3'-吲哚]-2'(1'H)-酮合成路线 （共 46 条）
反应条件
1: MCPBA
2: AlCl3 / CH2Cl2
3: CrO3
4: SOCl2
5: NH3
6: 39 percent / KH / bis-(2-methoxy-ethyl) ether / 2 h / Heating
View Scheme
参考文献
Fleming, Ian; Loreto, Maria Antonietta; Michael, Joseph P.; Wallace, Ian H. M.
Tetrahedron Letters, 1982 , vol. 23, # 19 p. 2053 - 2056
反应条件
1: AlCl3 / CH2Cl2
2: CrO3
3: SOCl2
4: NH3
5: 39 percent / KH / bis-(2-methoxy-ethyl) ether / 2 h / Heating
View Scheme
参考文献
Fleming, Ian; Loreto, Maria Antonietta; Michael, Joseph P.; Wallace, Ian H. M.
Tetrahedron Letters, 1982 , vol. 23, # 19 p. 2053 - 2056
反应条件
1: SOCl2
2: NH3
3: 39 percent / KH / bis-(2-methoxy-ethyl) ether / 2 h / Heating
View Scheme
参考文献
Fleming, Ian; Loreto, Maria Antonietta; Michael, Joseph P.; Wallace, Ian H. M.
Tetrahedron Letters, 1982 , vol. 23, # 19 p. 2053 - 2056
反应条件
2: MCPBA
3: TFA / CH2Cl2 / 15 h / 20 °C
4: CrO3
5: SOCl2
6: NH3
7: 39 percent / KH / bis-(2-methoxy-ethyl) ether / 2 h / Heating
View Scheme
参考文献
Fleming, Ian; Loreto, Maria Antonietta; Michael, Joseph P.; Wallace, Ian H. M.
Tetrahedron Letters, 1982 , vol. 23, # 19 p. 2053 - 2056
反应条件
1: acetic acid / 60 °C
2: mCPBA / CH2Cl2 / 1 h / 20 °C
View Scheme
参考文献
Liu, Kevin G.; Robichaud, Albert J.
Tetrahedron Letters, 2007 , vol. 48, # 3 p. 461 - 463
反应条件
1: acetic acid / 60 °C
2: mCPBA / CH2Cl2 / 1 h / 20 °C
View Scheme
参考文献
Liu, Kevin G.; Robichaud, Albert J.
Tetrahedron Letters, 2007 , vol. 48, # 3 p. 461 - 463
反应条件
1: NH3
2: 39 percent / KH / bis-(2-methoxy-ethyl) ether / 2 h / Heating
View Scheme
参考文献
Fleming, Ian; Loreto, Maria Antonietta; Michael, Joseph P.; Wallace, Ian H. M.
Tetrahedron Letters, 1982 , vol. 23, # 19 p. 2053 - 2056
反应条件
1: MCPBA
2: TFA / CH2Cl2 / 15 h / 20 °C
3: CrO3
4: SOCl2
5: NH3
6: 39 percent / KH / bis-(2-methoxy-ethyl) ether / 2 h / Heating
View Scheme
参考文献
Fleming, Ian; Loreto, Maria Antonietta; Michael, Joseph P.; Wallace, Ian H. M.
Tetrahedron Letters, 1982 , vol. 23, # 19 p. 2053 - 2056
反应条件
1: CrO3
2: SOCl2
3: NH3
4: 39 percent / KH / bis-(2-methoxy-ethyl) ether / 2 h / Heating
View Scheme
参考文献
Fleming, Ian; Loreto, Maria Antonietta; Michael, Joseph P.; Wallace, Ian H. M.
Tetrahedron Letters, 1982 , vol. 23, # 19 p. 2053 - 2056
反应条件
1: TFA / CH2Cl2 / 15 h / 20 °C
2: CrO3
3: SOCl2
4: NH3
5: 39 percent / KH / bis-(2-methoxy-ethyl) ether / 2 h / Heating
View Scheme
参考文献
Fleming, Ian; Loreto, Maria Antonietta; Michael, Joseph P.; Wallace, Ian H. M.
Tetrahedron Letters, 1982 , vol. 23, # 19 p. 2053 - 2056
