5-苯基-1,3-环己二酮合成路线 (共 57 条)
参考文献
Vorlaender; Knoetzsch
Justus Liebigs Annalen der Chemie, 1897 , vol. 294, p. 332
参考文献
Knoevenagel
Chemische Berichte, 1894 , vol. 27, p. 2341
Justus Liebigs Annalen der Chemie, 1896 , vol. 289, p. 167
反应条件
1: 5-phenylcyclohexane-1,3-dione With ammonium acetate in ethanol T=20°C; 7 h; Heating / reflux; 2: propynoic acid ethyl ester in ethanol T=20°C; 15.5 h; Heating / reflux;
参考文献
Takeda Chemical Industries, Ltd.
Patent: US6350749 B1, 2002 ;
Location in patent: Page column 65 ;
反应条件
chloroform; phosphorus pentachloride
参考文献
Hinkel; Hey
Journal of the Chemical Society, 1928 , p. 2787,2789
反应条件
acetic anhydride; diborane in diethylene glycol dimethyl ether
参考文献
Dunkelblum,E. et al.
Tetrahedron, 1972 , vol. 28, p. 1009 - 1024
参考文献
Vorlaender; Kohlmann
Chemische Berichte, 1899 , vol. 32, p. 1879
Justus Liebigs Annalen der Chemie, 1902 , vol. 322, p. 249
反应条件
permanganate(VII) ion
参考文献
Boyd; Clifford; Probert
Journal of the Chemical Society, 1920 , vol. 117, p. 1388
反应条件
Fremy’s salt; sodium acetate in water
参考文献
Teuber, Hans-Joachim; Hohn, Juergen; Gholami, Abbas
Chemische Berichte, 1983 , vol. 116, # 4 p. 1309 - 1319
反应条件
piperidine in ethanol 1 h, RT; 12 h, reflux;
参考文献
Afsah, E. M.; Sarhan, A. A.; Ibrahim, M. R.
Journal fuer Praktische Chemie (Leipzig), 1984 , vol. 326, # 4 p. 683 - 685
参考文献
Ionescu; Georgescu
Bulletin de la Societe Chimique de France, 1927 , vol. <4> 41, p. 705