N-(2-硝基苯基)乙醇胺合成路线 （共 20 条）
反应条件
1: H2 / Pd/C 2: 30 percent / K2CO3; [Cp*IrCl2]2 / xylene / 120 h / 140 °C View Scheme
参考文献
Ramage; Trappe
Journal of the Chemical Society, 1952 , p. 4406,4408
反应条件
1: Na2S2; H2O 2: concentrated aqueous HCl / 150 - 160 °C 3: palladium/charcoal / 150 °C / 0 Torr View Scheme
参考文献
Journal of the Chemical Society, , p. 4406,4408
反应条件
ammonium hydroxide; sodium sulfite in methanol T=70°C; 144 h;
参考文献
Forlani, Luciano; Boga, Carla; Mazza, Milena; Cavrini, Vanni; Andrisano, Vincenza
Tetrahedron, 1998 , vol. 54, # 18 p. 4647 - 4654
反应条件
1: 91 percent / HCOONH4 / Pd/C / methanol / 25 °C 2: boric acid / acetic acid / 1 h / 50 °C View Scheme
参考文献
Li, Wen-Shan; Zhang, Nanjing; Sayre, Lawrence M.
Tetrahedron, 2001 , vol. 57, # 21 p. 4507 - 4522
反应条件
1: 55.5 percent / NaH in oil / dimethylformamide / 30 - 35 °C 2: Zn; HCl 3: Heating View Scheme
参考文献
Goeker, Hakan; Ayhan-Kilcigil, Guelguen; Tuncbilek, Meral; Kus, Canan; Ertan, Rahmiye; Kendi, Engin; Oezbey, Sueheyla; Fort, Merce; Garcia, Celia; Farre, Antonio J.
Heterocycles, 1999 , vol. 51, # 11 p. 2561 - 2573
反应条件
1: 55.5 percent / NaH in oil / dimethylformamide / 30 - 35 °C
2: Zn; HCl
3: Heating
4: POCl3
View Scheme
参考文献
Goeker, Hakan; Ayhan-Kilcigil, Guelguen; Tuncbilek, Meral; Kus, Canan; Ertan, Rahmiye; Kendi, Engin; Oezbey, Sueheyla; Fort, Merce; Garcia, Celia; Farre, Antonio J.
Heterocycles, 1999 , vol. 51, # 11 p. 2561 - 2573
反应条件
sodium hydride in N,N-dimethyl-formamide
T=30 - 35°C; Alkylation;
参考文献
Goeker, Hakan; Ayhan-Kilcigil, Guelguen; Tuncbilek, Meral; Kus, Canan; Ertan, Rahmiye; Kendi, Engin; Oezbey, Sueheyla; Fort, Merce; Garcia, Celia; Farre, Antonio J.
Heterocycles, 1999 , vol. 51, # 11 p. 2561 - 2573
反应条件
1: 55.5 percent / NaH in oil / dimethylformamide / 30 - 35 °C
2: Zn; HCl
View Scheme
参考文献
Goeker, Hakan; Ayhan-Kilcigil, Guelguen; Tuncbilek, Meral; Kus, Canan; Ertan, Rahmiye; Kendi, Engin; Oezbey, Sueheyla; Fort, Merce; Garcia, Celia; Farre, Antonio J.
Heterocycles, 1999 , vol. 51, # 11 p. 2561 - 2573
反应条件
hydrogen; palladium on activated charcoal in ethanol
0.5 h; Ambient temperature;
参考文献
Sasho; Obase; Ichikawa; Kitazawa; Nonaka; Yoshizaki; Ishii; Shuto
Journal of Medicinal Chemistry, 1993 , vol. 36, # 5 p. 572 - 579
反应条件
sodium hydroxide in ethanol
参考文献
American Home Products Corporation
Patent: US5149700 A1, 1992 ;
