8-甲氧基-1,4-萘醌合成路线 （共 40 条）
反应条件
dihydrogen peroxide; iron powder
Multistep reaction;
参考文献
Wurm; Geres
Archiv der Pharmazie, 1984 , vol. 317, # 3 p. 278 - 280
反应条件
hydrogenchloride; sodium azide in methanol; water
12 h; Ambient temperature;
参考文献
Couladouros, Elias A.; Plyta, Zoi F.; Haroutounian, Serkos A.; Papageorgiou, Vassilios P.
Journal of Organic Chemistry, 1997 , vol. 62, # 1 p. 6 - 10
反应条件
ammonia in methanol
24 h;
参考文献
Arnone, Alberto; Merlini, Lucio; Nasini, Gianluca; De Pava, Orso Vajna
Synthetic Communications, 2007 , vol. 37, # 15 p. 2569 - 2577
反应条件
trimethylsilylazide in N,N-dimethyl-formamide
T=80°C; 3 h;
参考文献
Husu, Breda; Kafka, Stanislav; Kadunc, Zdenka; Tisler, Miha
Monatshefte fuer Chemie, 1988 , vol. 119, p. 215 - 222
反应条件
sodium dithionite; water in ethyl acetate
0.5 h;
参考文献
Qabaja; Jones
The Journal of organic chemistry, 2000 , vol. 65, # 21 p. 7187 - 7194
反应条件
Fe2(S04)3; sulfuric acid
2 h; Heating; Yield given;
参考文献
Wurm; Geres
Archiv der Pharmazie, 1989 , vol. 322, # 3 p. 155 - 157
反应条件
1: 1,4-dihydro-1,4-dioxo-5-methoxynaphthalene With sodium dithionite
Reduction;
2: dimethyl sulfate With potassium carbonate in diethyl ether
Methylation;
参考文献
Qabaja, Ghassan; Jones, Graham B.
Tetrahedron Letters, 2000 , vol. 41, # 28 p. 5317 - 5320
反应条件
sodium dithionite; potassium carbonate; acetone; dimethyl sulfate
Yield given. Multistep reaction;
参考文献
Zhang, Heping; Zembower, David E.; Chen, Zhidong
Bioorganic and Medicinal Chemistry Letters, 1997 , vol. 7, # 20 p. 2687 - 2690
反应条件
sodium dithionite; potassium carbonate
1.) dichloromethane, diethyl ether, water, 2.) dry aceton, reflux, 5 h; Yield given. Multistep reaction;
参考文献
Chorn, Trevor A.; Giles, Robin G.F.; Green, Ivan R.; Hugo, Victor I.; Mitchell, Peter R.K.; Yorke, Selwyn C.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , p. 1339 - 1343
反应条件
Fe2(S04)3; sulfuric acid
2 h; Heating; Yield given;
参考文献
Wurm; Geres
Archiv der Pharmazie, 1989 , vol. 322, # 3 p. 155 - 157
