8-甲氧基-1,4-萘醌合成路线 （共 40 条）
反应条件
P=0.5 Torr; (heating);
参考文献
Birch,A.J. et al.
Journal of the Chemical Society, 1964 , p. 2941 - 2944
反应条件
1: Ag2O
2: 0.5 Torr / (heating)
View Scheme
参考文献
Birch,A.J. et al.
Journal of the Chemical Society, 1964 , p. 2941 - 2944
反应条件
1: aq. KHCO3
2: Ag2O
3: 0.5 Torr / (heating)
View Scheme
参考文献
Birch,A.J. et al.
Journal of the Chemical Society, 1964 , p. 2941 - 2944
反应条件
ammonium cerium(IV) nitrate; water in acetonitrile
Mechanism;
参考文献
Laatsch, Hartmut
Liebigs Annalen der Chemie, 1986 , # 10 p. 1655 - 1668
反应条件
1: (i) KOH, (electrochemical oxidation), (ii) CF3CO2H, Et2O
2: (i) KOH, MeOH, (electrochemical oxidation), (ii) aq. AcOH, THF
View Scheme
参考文献
Jackson,D.K.; Swenton,J.S.
Synthetic Communications, 1977 , vol. 7, # 5 p. 333 - 337
参考文献
Maiti, Bhim C.; Musgrave, Oliver C.; Skoyles, Douglas
Tetrahedron, 2005 , vol. 61, # 27 p. 6568 - 6574
反应条件
dihydrogen peroxide; iron powder
Multistep reaction;
参考文献
Wurm; Geres
Archiv der Pharmazie, 1984 , vol. 317, # 3 p. 278 - 280
反应条件
bromine in acetic acid
Ambient temperature;
参考文献
Cameron, Donald W.; Feutrill, Geoffrey I.; Griffiths, Peter G.
Australian Journal of Chemistry, 1981 , vol. 34, # 7 p. 1513 - 1522
反应条件
1: 64 percent / AgNO3; aq. (NH4)2S28 / acetonitrile / 2 h / 75 °C
2: 94 percent / benzylidenebis(tricyclohexylphosphine)dichlororuthenium / toluene / 24 h / 20 - 100 °C
3: 92 percent / Pd/C / toluene / Heating
View Scheme
参考文献
Chigr; Fillion; Rougny; Berlion; Riondel; Beriel
Chemical and Pharmaceutical Bulletin, 1990 , vol. 38, # 3 p. 688 - 691
反应条件
dihydrogen peroxide
1.) dioxan, room temp., 30 min, 2.) dioxan, 15 min; Yield given. Multistep reaction;
参考文献
Wurm, Gotthard; Geres, Uwe
Archiv der Pharmazie (Weinheim, Germany), 1984 , vol. 317, # 7 p. 606 - 609
