N-[(4-氯苯基氨基)(硫代羰基)]苯甲酰胺合成路线 (共 9 条)
反应条件
hydrazine T=25°C; 0.166667 h;
参考文献
Kodomari, Mitsuo; Suzuki, Masato; Tanigawa, Keiko; Aoyama, Tadashi
Tetrahedron Letters, 2005 , vol. 46, # 35 p. 5841 - 5843
反应条件
2,6-dichloro-N-hydroxybenzenecarboximidoyl chloride; triethylamine in tetrahydrofuran 0.166667 h; Ambient temperature;
参考文献
Synthetic Communications, , vol. 28, # 10 p. 1879 - 1884
参考文献
Upadhyaya Srivastava
Journal of the Indian Chemical Society, 1982 , vol. 59, # 6 p. 767 - 768
反应条件
1: ammonium thiocyanate; benzoyl chloride in acetone
0.25 h; Heating;
2: 4-chloro-aniline in acetone
0.5 h; Heating;
参考文献
Holla, B. Shivarama; Malini; Rao, B. Sooryanarayana; Sarojini; Kumari, N. Suchetha
European Journal of Medicinal Chemistry, 2003 , vol. 38, # 3 p. 313 - 318
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Narayana; Ashalatha; Vijaya Raj; Suchetha Kumari
Phosphorus, Sulfur and Silicon and the Related Elements, 2006 , vol. 181, # 6 p. 1381 - 1389
反应条件
1: PEG-400 / 5 h / 20 °C
2: 5 h / 20 °C
View Scheme
参考文献
Wei, Tai-Bao; Lin, Qi; Zhang, You-Ming; Wei, Wei
Journal of Chemical Research - Part S, 2003 , # 10 p. 666 - 667
反应条件
1: thionyl chloride / N,N-dimethyl-formamide
2: tetrahydrofuran
3: tetrahydrofuran / 0.17 h / 60 - 65 °C / |Microwave irradiation
View Scheme
参考文献
Rauf, Muhammad Khawar; Talib, Ammara; Badshah, Amin; Zaib, Sumera; Shoaib, Khurram; Shahid, Mohammad; Floerke, Ulrich; Imtiaz-Ud-Din; Iqbal, Jamshed
European Journal of Medicinal Chemistry, 2013 , vol. 70, p. 487 - 496
反应条件
1: 85 percent / 2,5 N NaOH / 100 °C
2: 65 percent / methanol / Heating
3: 55 percent / 20 h / 140 °C
View Scheme
参考文献
Gupta, K. A.; Saxena, Anil K.; Jain, Padam C.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 3 p. 228 - 233
反应条件
2,6-dichloro-N-hydroxybenzenecarboximidoyl chloride; triethylamine in tetrahydrofuran
0.166667 h; Ambient temperature;
参考文献
Jung, Keum Shin; Lee, Hong Jung; Song, Hyun Nam; Kim, Jae Nyoung
Synthetic Communications, 1998 , vol. 28, # 10 p. 1879 - 1884
反应条件
Spirolt;cyclohexan-1,3'-oxaziridingt; in toluene
T=20 - 25°C; 4 h;
参考文献
Andreae, Siegfried; Schmitz, Ernst
Journal fuer Praktische Chemie (Leipzig), 1987 , vol. 329, # 6 p. 1008 - 1014