3,3',4,4'-四甲基联苯合成路线 (共 29 条)
反应条件
sodium hydroxide; hydrazine hydrate; mercury dichloride; palladium dichloride 6 h; Heating;
参考文献
Nakajima, Riichiro; Shintani, Yuji; Hara, Tadashi
Bulletin of the Chemical Society of Japan, 1980 , vol. 53, # 6 p. 1767 - 1768
反应条件
3,4-dimethyliodobenzene; copper T=270°C; 0.0833333 h;
参考文献
Bushby, Richard J.; Hardy, Cristopher
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 721 - 724
反应条件
Pd0(tris(tert-butyl)phosphine)2; [(pentamethylcyclopentadiene)(PMe3)IrMeCl]; potassium tetrakis(pentafluorophenyl)-borate in water T=100°C; 16 h; Inert atmosphere; regioselective reaction;
参考文献
Durak, Landon J.; Lewis, Jared C.
Organometallics, 2014 , vol. 33, # 3 p. 620 - 623
反应条件
copper T=270°C; 0.0833333 h;
参考文献
Bushby, Richard J.; Hardy, Cristopher
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 721 - 724
反应条件
4-iodoveratrole; copper T=270°C; 0.0833333 h;
参考文献
Bushby, Richard J.; Hardy, Cristopher
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 721 - 724
反应条件
copper T=270°C; 0.0833333 h;
参考文献
Bushby, Richard J.; Hardy, Cristopher
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 721 - 724
反应条件
3,4-dimethyliodobenzene; copper T=235 - 280°C;
参考文献
Bushby, Richard J.; Hardy, Cristopher
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 721 - 724
反应条件
1: 35 percent / copper powder / 235 - 280 °C 2: 88 percent / iodic acid, iodine / acetic acid / 7 h / Heating 3: copper powder, 1-iodo-3,4-dimethylbenzene / 0.08 h / 270 °C View Scheme
参考文献
Bushby, Richard J.; Hardy, Cristopher
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 721 - 724
反应条件
1: 88 percent / iodic acid, iodine / acetic acid / 7 h / Heating 2: copper powder / 0.08 h / 270 °C View Scheme
参考文献
Bushby, Richard J.; Hardy, Cristopher
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 721 - 724
反应条件
copper T=235 - 280°C;
参考文献
Bushby, Richard J.; Hardy, Cristopher
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 721 - 724