3,3',4,4'-四甲基联苯合成路线 (共 29 条)
反应条件
[2,2']bipyridinyl; nickel; zinc; triphenylphosphine in N,N-dimethyl-formamide T=90°C; 24 h;
参考文献
Kim, Hyung-Sun; Kim, Yun-Hi; Ahn, Seung-Kuk; Kwon, Soon-Ki
Macromolecules, 2003 , vol. 36, # 7 p. 2327 - 2332
反应条件
nickel in N,N-dimethyl-formamide T=140°C; 23 h;
参考文献
Chao, C. S.; Cheng, C. H.; Chang, C. T.
Journal of Organic Chemistry, 1983 , vol. 48, # 25 p. 4904 - 4907
反应条件
[2,2']bipyridinyl; oxygen; iron(III) chloride in tetrahydrofuran T=20°C; 0.166667 h;
参考文献
Liu, Wei; Lei, Aiwen
Tetrahedron Letters, 2008 , vol. 49, # 4 p. 610 - 613
反应条件
sodium hydroxide; sodium formate; N-hexadecyl-N,N,N-trimethylammonium bromide; palladium on activated charcoal in water T=110°C; Dehalogenation; coupling; 4 h;
参考文献
Mukhopadhyay, Sudip; Rothenberg, Gadi; Wiener, Harold; Sasson, Yoel
Tetrahedron, 1999 , vol. 55, # 51 p. 14763 - 14768
反应条件
chloroethylmethylchloride; anhydrous iron chloride in tetrahydrofuran T=30 - 50°C; 3 h; Product distribution / selectivity;
参考文献
Toray Fine Chemicals Co., Ltd.; Haqyashi, Tamio
Patent: EP2075241 A1, 2009 ;
Location in patent: Page/Page column 6-7 ;
反应条件
air in N,N-dimethyl-formamide T=20°C; 16 h; Green chemistry;
参考文献
Puthiaraj, Pillaiyar; Suresh, Palaniswamy; Pitchumani, Kasi
Green Chemistry, 2014 , vol. 16, # 5 p. 2865 - 2875
反应条件
dilithium tetrachloropalladate in tetrahydrofuran 5 h; Heating;
参考文献
Kjonaas, Richard A.; Shubert, David C.
Journal of Organic Chemistry, 1983 , vol. 48, # 11 p. 1924 - 1925
反应条件
lead(IV) acetate; trifluoroacetic acid in dichloromethane
参考文献
Kozhevnikov, I. V.; Kim. V. I.; Talzi, E. P.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1985 , vol. 34, # 10 p. 2001 - 2007
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1985 , # 10 p. 2167 - 2174
反应条件
2-fluoro-pyridine; oxygen; palladium diacetate; copper(II) bis(trifluoromethanesulfonate); trifluoroacetic acid in acetic acid T=80°C; P=760.051 Torr; 17 h; regioselective reaction;
参考文献
Izawa, Yusuke; Stahl, Shannon S.
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 18 p. 3223 - 3229
反应条件
4-iodoveratrole; copper T=235 - 280°C;
参考文献
Bushby, Richard J.; Hardy, Cristopher
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 721 - 724