2,3-二氢-1,1-二甲基-1H-茚合成路线 (共 48 条)
反应条件
reagiert analog wie das Toluol;
参考文献
Schaap; Pines
Journal of the American Chemical Society, 1957 , vol. 79, p. 4967,4968
反应条件
phosphoric acid, fully deuterated
T=230 - 240°C; 3 h; Yield given. Title compound not separated from byproducts;
参考文献
Sakhabutdinov, A. G.; Usmanova, A. G.; Frolov, P. A.; Kushnarev, D. F.; Schmidt, F. K.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 8 p. 1452 - 1455
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 8 p. 1610 - 1614
反应条件
phosphoric acid, fully deuterated
T=230 - 240°C; 3 h; Yield given. Title compound not separated from byproducts;
参考文献
Sakhabutdinov, A. G.; Usmanova, A. G.; Frolov, P. A.; Kushnarev, D. F.; Schmidt, F. K.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 8 p. 1452 - 1455
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 8 p. 1610 - 1614
反应条件
in methanol
T=20°C; 65 h; electrolysis; Hg cathode, platinum anode; -1.8 V vs SCE; 0.1 mol/l Ba(ClO4)2;
参考文献
Ismail, M. T.; Abdel-Wahab, A. A.; Mohamed, O. S.; Khalaf, A. A.
Bulletin de la Societe Chimique de France, 1985 , # 6 p. 1174 - 1176
反应条件
sulfuric acid in benzene
T=22°C; 3 h; other concentration of H2SO4, time, and solvents, also alkylating agents; var. indanes; Product distribution;
参考文献
Eisenbraun, Edmund J.; Harms, Weldon M.; Palaniswamy, Venkatapuram A.; Chen, Hoffman H.; Porcaro, Peter J.; et al.
Journal of Organic Chemistry, 1982 , vol. 47, # 2 p. 342 - 346
参考文献
Closson et al.
Journal of Organic Chemistry, 1957 , vol. 22, p. 646
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Podall; Foster
Journal of Organic Chemistry, 1958 , vol. 23, p. 401
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Pines et al.
Journal of the American Chemical Society, 1955 , vol. 77, p. 554,555
Full Text Show Details
Schaap; Pines
Journal of the American Chemical Society, 1957 , vol. 79, p. 4967,4968
反应条件
phosphorus pentachloride; arsenium trifluoride
1.) rt, 3 d, 2.) 10 deg C; Yield given. Multistep reaction;
参考文献
Fridland, S. V.; Miftakhov, M. N.
J. Gen. Chem. USSR (Engl. Transl.), 1988 , vol. 58, # l p. 41 - 46,35 - 39
参考文献
Bogert; Davidson
Journal of the American Chemical Society, 1934 , vol. 56, p. 185,187
参考文献
Bogert; Davidson
Journal of the American Chemical Society, 1934 , vol. 56, p. 185,187
反应条件
(i) NaH, THF, (ii) (pyrolysis); Multistep reaction;
参考文献
Sekiguchi,A.; Ando,W.
Bulletin of the Chemical Society of Japan, 1977 , vol. 50, p. 3067 - 3068