1,5,9-环十二烷三烯合成路线 （共 25 条）
反应条件
ethyl aluminum sesquichloride; water; titanium tetrachloride in benzene T=60°C; P=1500.15 Torr; Product distribution / selectivity;
参考文献
DEGUSSA AG
Patent: US2007/265184 A1, 2007 ;
Location in patent: Page/Page column 4 ;
反应条件
iron (III) acetylacetonate; PC-P(OBu-t)2; triethylaluminum in benzene T=50°C; 1 h; Product distribution; Pressure (range begins): 730 <unit not given>;
参考文献
Potapov, G. P.; Punegov, V. V.; Dzhemilev, U. M.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1985 , vol. 34, # 7 p. 1342 - 1345
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1985 , # 7 p. 1468 - 1471
反应条件
Ni acetylacetonate; triethylaluminum; triphenylphosphine in toluene T=90°C; 1.41667 h; other temperature; various ratio of components. Other object of study: the rate constants; KineticsMechanismProduct distribution;
参考文献
Akhmedov, V. M.; Khanmetov, A. A.; Azizov, A. G.
Journal of Organic Chemistry USSR (English Translation), 1981 , p. 1479 - 1485
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 8 p. 1661 - 1668
反应条件
iron (III) acetylacetonate; C17H34O2P2; triethylaluminum in benzene T=50°C; 4 h; Product distribution; Pressure (range begins): 730 <unit not given>;
参考文献
Potapov, G. P.; Punegov, V. V.; Dzhemilev, U. M.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1985 , vol. 34, # 7 p. 1342 - 1345
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1985 , # 7 p. 1468 - 1471
反应条件
tert.-butylhydroperoxide T=165°C; copolymerization; 24 h; Product distribution; Further Variations:ReagentsTemperatures;
参考文献
Nikulin; Filimonova
Russian Journal of Applied Chemistry, 2000 , vol. 73, # 1 p. 157 - 161
反应条件
T=80°C; 5 h; also in presence aprotic solvents, var, times, temp.; Product distribution;
参考文献
Grenouillet, P.; Neibecker, D.; Tkatchenko, I.
Journal of Organometallic Chemistry, 1983 , vol. 243, # 2 p. 213 - 222
反应条件
sodium mono-oxide Product distribution / selectivity;
参考文献
BASF SE; Teles, Joaquim Henrique; Baumann, Dieter; Röβler-Feigel, Beatrice
Patent: US8404901 B2, 2013 ;
Location in patent: Page/Page column 26; 27 ;
反应条件
Nitrous oxide T=280°C; P=75007.5 Torr; Product distribution / selectivity;
参考文献
BASF SE
Patent: US2010/191018 A1, 2010 ;
Location in patent: Page/Page column 17 ;
反应条件
1: dihydrogen peroxide / H3[PW12O40]; Aliquatreg; 336 / water 2: hydrogen / platinum on activated charcoal 3: lithium iodide / 230 °C 4: hydroxylammonium sulphate; ammonia; sulfuric acid; ammonium sulfate / toluene; water / 85 °C / pH 4 - 5.8 / Industry scale 5: thionyl chloride; zinc(II) chloride / toluene / 0.42 h / 105 °C View Scheme
参考文献
UBE INDUSTRIES, LTD.
Patent: US2013/5960 A1, 2013 ;
反应条件
oxygen T=100°C; P=5931.67 Torr; Product distribution / selectivity;
参考文献
US2009/240068 A1, ;
Page/Page column 5 ;
