1: 93 percent / K2CO3 / dimethylformamide / 20 h / 100 °C
2: 65.6 percent / LiAlH4 / tetrahydrofuran / 1.5 h / Ambient temperature
3: 88.8 percent / SOCl2 / benzene; CH2Cl2; pyridine / below 10 deg C, then 4 deg C, 1 h
View Scheme
参考文献
Hill, Robert A.; Carter, Rachel H.; Staunton, James
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2570 - 2576
1: K2CO3*1.5H2O / acetone / 24 h / Heating
2: 1.99 g / NaOH / methanol; H2O / 3 h / Heating
View Scheme
参考文献
Hill, Robert A.; Carter, Rachel H.; Staunton, James
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2570 - 2576
Hill, Robert A.; Carter, Rachel H.; Staunton, James
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2570 - 2576