3,5-二苯基-2-异恶唑啉合成路线 （共 45 条）
参考文献
Surov, Igor; Lund, Henning
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1986 , vol. 40, # 10 p. 831 - 838
反应条件
[Mo(CO)3(acetonitrile)3]; silica gel 1.) MeCN, room temp., 30 min, 2.) 16 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Guarna, Antonio; Guidi, Antonio; Goti, Andrea; Brandi, Alberto; Sarlo, Francesco De
Synthesis, 1989 , # 3 p. 175 - 178
反应条件
Yield given. Multistep reaction;
参考文献
Grund, Hartmut; Jaeger, Volker
Liebigs Annalen der Chemie, 1980 , # 1 p. 80 - 100
反应条件
multistep reaction; selective N-O cleavage effected by Mo(CO)3(MeCN)3 or Mo(CO)6 and silica gel; Product distribution;
参考文献
Guarna, Antonio; Guidi, Antonio; Goti, Andrea; Brandi, Alberto; Sarlo, Francesco De
Synthesis, 1989 , # 3 p. 175 - 178
反应条件
lithium aluminium tetrahydride in diethyl ether Ambient temperatureovernight; Yields of byproduct given;
参考文献
Jaeger, Volker; Buss, Volker
Liebigs Annalen der Chemie, 1980 , # 1 p. 101 - 121
反应条件
1: With borane dimethyl sulfide complex in dichloromethane; toluene T=20°C; 46 h; Inert atmosphere; 2: With triethylamine in ethanol 2 h; Inert atmosphereReflux; optical yield given as percent dediastereoselective reaction;
参考文献
Tokizane, Masashi; Sato, Kaori; Ohta, Tetsuo; Ito, Yoshihiko
Tetrahedron Asymmetry, 2008 , vol. 19, # 21 p. 2519 - 2528
反应条件
Oxonereg;; potassium chloride in water
T=20°C; 3 h; Green chemistry; Reagent/catalystSolvent;
参考文献
Han, Liuquan; Zhang, Bijun; Zhu, Min; Yan, Jie
Tetrahedron Letters, 2014 , vol. 55, # 14 p. 2308 - 2311
反应条件
1,4-diaza-bicyclo[2.2.2]octane in chloroform
T=60°C; 40 h;
参考文献
Cecchi, Luca; De Sarlo, Francesco; Machetti, Fabrizio
European Journal of Organic Chemistry, 2006 , # 21 p. 4852 - 4860
反应条件
sodium nitrite in chloroform; trifluoroacetic acid
T=0°C; 0.5 h;
参考文献
Shabarov, Yu. S.; Saginova, L. G.; Gazzaeva, R. A.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, p. 2319 - 2320
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 12 p. 2627 - 2628
反应条件
potassium carbonate in N,N-dimethyl-formamide
T=140°C; 2 h; Inert atmosphere;
参考文献
Zhu, Xu; Wang, Yi-Feng; Ren, Wei; Zhang, Feng-Lian; Chiba, Shunsuke
Organic Letters, 2013 , vol. 15, # 13 p. 3214 - 3217
