sodium hydride in N,N-dimethyl-formamide
T=0°C; 0.75 h;
参考文献
Al-Zaidi, Shakir M.R.; Crilley, Martine M. L.; Stoodley, Richard J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 2259 - 2266
1: 23 percent / pyridine / 48 h / 0 °C
2: 77 percent / NaH / dimethylformamide / 0.75 h / 0 °C
View Scheme
参考文献
Al-Zaidi, Shakir M.R.; Crilley, Martine M. L.; Stoodley, Richard J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 2259 - 2266
1: 87 percent / HBr / acetic acid / 0.5 h
2: 52 percent / pyridine / 12 h
3: 77 percent / NaH / dimethylformamide / 0.75 h / 0 °C
View Scheme
参考文献
Al-Zaidi, Shakir M.R.; Crilley, Martine M. L.; Stoodley, Richard J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 2259 - 2266
1: DCC / CH2Cl2 / 1 h / 0 °C
2: 87 percent / HBr / acetic acid / 0.5 h
3: 52 percent / pyridine / 12 h
4: 77 percent / NaH / dimethylformamide / 0.75 h / 0 °C
View Scheme
参考文献
Al-Zaidi, Shakir M.R.; Crilley, Martine M. L.; Stoodley, Richard J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 2259 - 2266
1: 52 percent / pyridine / 12 h
2: 77 percent / NaH / dimethylformamide / 0.75 h / 0 °C
View Scheme
参考文献
Al-Zaidi, Shakir M.R.; Crilley, Martine M. L.; Stoodley, Richard J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 2259 - 2266
1: 84 percent Spectr. / 1M hydrochloric acid / acetone / 2 h
2: 59 percent / Et3N / CH2Cl2 / 12 h
3: 62 percent / tetrahydrofuran / 0.5 h
4: 75 percent / pyridine / 12 h / Ambient temperature
5: 77 percent / NaH / dimethylformamide / 0.75 h / 0 °C
View Scheme
参考文献
Al-Zaidi, Shakir M.R.; Crilley, Martine M. L.; Stoodley, Richard J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 2259 - 2266
