2-乙酰氨基-2-脱氧-3-o-(beta-d-氟代半乳糖)-d-吡喃葡萄糖合成路线 (共 2 条)
反应条件
1.1: pyridine / 50 °C 2.1: acetyl chloride / methanol / 0 - 20 °C / |Inert atmosphere 3.1: potassium carbonate; tetra(n-butyl)ammonium hydrogensulfate / water; dichloromethane / 20 °C 4.1: sodium methylate / methanol 4.2: Amberlite IR-120 (H+) resin View Scheme
参考文献
Boettcher, Stephan; Thiem, Joachim
RSC Advances, 2014 , vol. 4, # 21 p. 10856 - 10861
反应条件
T=37°C; MnCl2, NaCl, CTP, Triton X-100, sialyltransferase; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Lubineau, Andre; Auge, Claudine; Francois, Patrice
Carbohydrate Research, 1992 , vol. 228, # 1 p. 137 - 144