2,6-二叔丁基-4-甲氧基苯酚合成路线 (共 56 条)
反应条件
sulfuric acid; Petroleum ether T=50°C; Einleiten von 2-Methyl-propen;
参考文献
Sears; Kitchen
Journal of the American Chemical Society, 1949 , vol. 71, p. 4110
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Mueller; Ley
Chemische Berichte, 1955 , vol. 88, p. 601,612
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Cook et al.
Journal of the American Chemical Society, 1955 , vol. 77, p. 1672
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Ingold
Canadian Journal of Chemistry, 1960 , vol. 38, p. 1092,1093
反应条件
sodium hydroxide T=90 - 100°C; 1.5 h;
参考文献
Dobronravova, Z. A.; Meshcheryakov, V. I.; Prishchenko, Yu. E.; Gavrilov, L. D.; Vereshchagin, L. I.
Journal of Organic Chemistry USSR (English Translation), 1980 , p. 910 - 914
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 5 p. 1034 - 1039
反应条件
(3,5-di-tert-butyl-4-oxo-2,5-cyclohexadien-1-ylidene)-(3,5-di-tert-butyl-4-hydroxyphenyl)methane in toluene T=24.9°C; Equilibrium constant;
参考文献
Lucarini, Marco; Mugnaini, Veronica; Pedulli, Gian Franco; Guerra, Maurizio
Journal of the American Chemical Society, 2003 , vol. 125, # 27 p. 8318 - 8329
参考文献
Pospisil,J. et al.
Collection of Czechoslovak Chemical Communications, 1966 , vol. 31, p. 98 - 105
反应条件
1: 210 °C / Erwaermen des Reaktionsprodukts in Petrolaether mit Zink-Pulver und Essigsaeure 2: aqueous NaOH View Scheme
参考文献
Cook et al.
Journal of the American Chemical Society, 1955 , vol. 77, p. 1672
反应条件
sulfuric acid 2 h; Ambient temperature;
参考文献
Brunow, G.; Karhu, M.
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1980 , vol. 34, # 10 p. 777 - 778
反应条件
bromine; silver perchlorate T=0°C; 0.05 h;
参考文献
Omura, Kanji
Journal of Organic Chemistry, 1996 , vol. 61, # 20 p. 7156 - 7161
反应条件
1.1: 99 percent / aq. NaOH / ethanol / 72 h / 25 °C 2.1: Et3N; DPPA / toluene; dimethylformamide / 3 h / Heating 2.2: 60 percent / H2O / toluene; dimethylformamide / Heating View Scheme
参考文献
Mirk, Daniela; Waldvogel, Siegfried R.
Tetrahedron Letters, 2004 , vol. 45, # 42 p. 7911 - 7914
反应条件
sodium hydroxide; dihydrogen peroxide in methanol
参考文献
Gierer,J. et al.
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1977 , vol. 31, p. 561 - 572
反应条件
silver perchlorate; sodium carbonate T=0°C; 0.0333333 h; Yield given. Yields of byproduct given;
参考文献
Omura, Kanji
Journal of Organic Chemistry, 1996 , vol. 61, # 20 p. 7156 - 7161