反应条件
1: 95 percent / lithium aluminum hydride / diethyl ether / 1) 10 deg C, 30 min, 2) 25 deg C, 1 h 2: 80 percent / chromic anhydride, pyridine / CH2Cl2 3: 1) Mg, 3) 30percent perchloric acid / 1) ether, 2) a) -5 deg C, 10 min, b) 30 min, 3) THF, 25 deg C, 2 h 4: 87 percent / H2 / 1percent Pd/CaCO3 / methanol / 0.1 h 5: TsOH*H2O / benzene / 5 h / Heating View Scheme
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 38, # 1.2 p. 131 - 134
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , vol. 38, # 1 p. 144 - 147
