2,4-二羟基-6-甲基苯甲醛合成路线 （共 25 条）
反应条件
potassium hydroxide; water
参考文献
Tiemann; Helkenberg
Chemische Berichte, 1879 , vol. 12, p. 1002
反应条件
(i) ZnCl2, Et2O, (ii) aq. HCl; Multistep reaction;
参考文献
Gross,H.; Matthey,G.
Chemische Berichte, 1964 , vol. 97, p. 2606 - 2613
参考文献
Grundmann; Richter
Chemische Berichte, 1966 , vol. 99, p. 2705
反应条件
sulfuryl dichloride in diethyl ether 1.) 0 deg C, 1.5 h, 2.) r.t., 8 h;
参考文献
Safaryn, J. E.; Chiarello, J.; Chen, K.-M.; Joullie, M. M.
Tetrahedron, 1986 , vol. 42, # 10 p. 2635 - 2642
反应条件
sodium chlorite; sodium dihydrogenphosphate in water; dimethyl sulfoxide
参考文献
UNIVERSITY OF IOWA RESEARCH FOUNDATION; JIN, Zhendong; KANG, Ying
Patent: WO2004/58738 A1, 2004 ;
Location in patent: Page 2/2; 10 ;
反应条件
hydrogenchloride; amalgamated zinc
参考文献
Ballantine,J.A. et al.
Phytochemistry (Elsevier), 1968 , vol. 7, p. 1529 - 1534
反应条件
acetic anhydride T=180°C; Erwaermen des Reaktionsprodukts mit wss.-aethanol. Natronlauge und anschliessend Ansaeuern;
参考文献
Balaiah et al.
Proceedings - Indian Academy of Sciences, Section A, 1942 , # 16 p. 68,77
反应条件
potassium carbonate in acetone 6 h; Heating;
参考文献
Wang, Ping; Zhang, Zhaojun; Yu, Biao
Journal of Organic Chemistry, 2005 , vol. 70, # 22 p. 8884 - 8889
反应条件
1: (i) K2CO3, acetone, (ii) Na<AlH2(OCH2CH2OMe)2> 2: H2 / PdO View Scheme
参考文献
Better,J.; Gatenbeck,S.
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1979 , vol. 33, p. 235 - 238
反应条件
potassium carbonate in acetone 5 h; Reflux;
参考文献
Merck Patent GmbH
Patent: US2010/16372 A1, 2010 ;
Location in patent: Page/Page column 12 ;
US 20100016372 A1
