2,4-二羟基-6-甲基苯甲醛合成路线 （共 25 条）
反应条件
1: With trichlorophosphate 2: With sodium hydroxide
参考文献
UNIVERSITY OF IOWA RESEARCH FOUNDATION; JIN, Zhendong; KANG, Ying
Patent: WO2004/58738 A1, 2004 ;
Location in patent: Page 2/2; 10 ;
反应条件
1: With hydrogenchloride in diethyl ether 2 h; Inert atmosphere; 2: With water T=100°C;
参考文献
THE UNIVERSITY OF SUSSEX; MOORE, Anthony Lennox; ALBURY, Mary Susan; YOUNG, Luke Edward; ELLIOTT, Catherine
Patent: WO2013/160670 A1, 2013 ;
Location in patent: Page/Page column 24 ;
反应条件
hydrogenchloride; aluminium trichloride; zinc cyanide in diethyl ether 2 h;
参考文献
Solladie; Rubio; Carreno; Ruano
Tetrahedron Asymmetry, 1990 , vol. 1, # 3 p. 187 - 198
反应条件
hydrogenchloride; diethyl ether Zersetzung des entstandenen salzsaeure Aldimids durch siedendes wasser;
参考文献
Gattermann; Koebner
Chemische Berichte, 1899 , vol. 32, p. 279
Full Text Show Details
Adams; Levine
Journal of the American Chemical Society, 1923 , vol. 45, p. 2377
参考文献
Statens Serum Institute
Patent: US2003/65039 A1, 2003 ;
参考文献
Pfau
Helvetica Chimica Acta, 1933 , vol. 16, p. 282,286
反应条件
1: diethyl ether / Einleiten von Chlorwasserstoff; Erwaermen des Reaktionsgemisches mit Wasser 2: sulfuric acid 3: copper / 250 °C View Scheme
参考文献
Pfau
Helvetica Chimica Acta, 1933 , vol. 16, p. 282,286
反应条件
1: sulfuric acid 2: copper / 250 °C View Scheme
参考文献
Pfau
Helvetica Chimica Acta, 1933 , vol. 16, p. 282,286
反应条件
hydrogenchloride; diethyl ether Spaltung des enstandenen Oxims mit verd. Schwefelsaeure;
参考文献
Ziegler
Patent: DE114195 ;
Full Text Show Details
Scholl; Bertsch
Chemische Berichte, 1901 , vol. 34, p. 1443
反应条件
hydroxylamine-o-sulphonic acid Spaltung des Reaktionsproduktes;
参考文献
Geigy and Co.
Patent: DE105798 ;
