1.1: 85 percent / Et3N; 1,3-dichlorocyclohexylcarbodiimide / CH2Cl2 / 20 °C 2.1: Mg / tetrahydrofuran / 1 h / 20 °C 2.2: 77 percent / tetrahydrofuran / -78 - 20 °C 3.1: Amberlyst 15; H2O / acetone / 4 h / 20 °C 3.2: 81 percent / Et3N / CH2Cl2 / 2 h / 20 °C 4.1: 98 percent / CH2Cl2; methanol / 1 h / 20 °C View Scheme
参考文献
Baxendale, Ian R.; Brusotti, Gloria; Matsuoka, Masato; Ley, Steven V.
Journal of the Chemical Society. Perkin Transactions 1, 2002 , vol. 2, # 2 p. 143 - 154
1.1: Mg / tetrahydrofuran / 1 h / 20 °C 1.2: 77 percent / tetrahydrofuran / -78 - 20 °C 2.1: Amberlyst 15; H2O / acetone / 4 h / 20 °C 2.2: 81 percent / Et3N / CH2Cl2 / 2 h / 20 °C 3.1: 98 percent / CH2Cl2; methanol / 1 h / 20 °C View Scheme
参考文献
Baxendale, Ian R.; Brusotti, Gloria; Matsuoka, Masato; Ley, Steven V.
Journal of the Chemical Society. Perkin Transactions 1, 2002 , vol. 2, # 2 p. 143 - 154
1.1: Amberlyst 15; H2O / acetone / 4 h / 20 °C 1.2: 81 percent / Et3N / CH2Cl2 / 2 h / 20 °C 2.1: 98 percent / CH2Cl2; methanol / 1 h / 20 °C View Scheme
参考文献
Baxendale, Ian R.; Brusotti, Gloria; Matsuoka, Masato; Ley, Steven V.
Journal of the Chemical Society. Perkin Transactions 1, 2002 , vol. 2, # 2 p. 143 - 154
Acheson, R. Morrin; Ferris, Michael J.; Critchley, Stephen R.; Watkin, David J.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1980 , p. 326 - 329
