1: With lithium aluminium tetrahydride in tetrahydrofuran; diethyl ether 3 h; Inert atmosphereReflux; 2: With Glauber's salt in tetrahydrofuran; diethyl ether
参考文献
Fustero, Santos; Moscardo, Javier; Sanchez-Rosello, Maria; Flores, Sonia; Guerola, Marta; Pozo, Carlos Del
Tetrahedron, 2011 , vol. 67, # 38 p. 7412 - 7417
1: With Grubb's 2nd generation catalyst in dichloromethane 6 h; Heating; 2: With hydrogen; acetic acid; palladium on activated charcoal in methanol T=30°C; P=760 Torr; 24 h; 3: With lithium aluminium tetrahydride in tetrahydrofuran 4 h; Heating; Title compound not separated from byproducts;
参考文献
Ma, Shengming; Ni, Bukuo
Chemistry - A European Journal, 2004 , vol. 10, # 13 p. 3286 - 3300
1: With Grubb's 2nd generation catalyst in dichloromethane 6 h; Heating; 2: With hydrogen; acetic acid; palladium on activated charcoal in methanol T=30°C; P=760 Torr; 24 h; 3: With lithium aluminium tetrahydride in tetrahydrofuran 4 h; Heating; Title compound not separated from byproducts;
参考文献
Ma, Shengming; Ni, Bukuo
Chemistry - A European Journal, 2004 , vol. 10, # 13 p. 3286 - 3300
