2-羟基-5-(2-甲基-2-丙基)-1,4-苯醌合成路线 （共 24 条）
反应条件
hydrazine in acetonitrile-D3 168 h;
参考文献
Lee; Jeon; Huang; Sayre
Journal of Organic Chemistry, 2001 , vol. 66, # 6 p. 1925 - 1937
反应条件
1: 40 percent / conc. aq. H2SO4 / 2 h / Heating 2: 17 percent / benzylamine / ethanol / 1 h / Heating View Scheme
参考文献
Mure, Minae; Klinman, Judith P.
Journal of the American Chemical Society, 1995 , vol. 117, # 34 p. 8698 - 8706
反应条件
in acetonitrile T=25°C; other amines; also benzylamine d2; MechanismRate constant;
参考文献
Mure, Minae; Klinman, Judith P.
Journal of the American Chemical Society, 1995 , vol. 117, # 34 p. 8707 - 8718
反应条件
in acetonitrile T=25°C; other solvent (DMSO); also with benzylamine-d2 and 5-amino-1,3-cyclohexadienecarboxylic acid; Mechanism;
参考文献
Lee Younghee; Sayre
Journal of the American Chemical Society, 1995 , vol. 117, # 48 p. 11823 - 11828
反应条件
sodium hydroxide; sodium metasilicate; diethylenetriamine-N,N,N',N'',N''-pentaacetic acid; dihydrogen peroxide 1.) water, 40 deg C, 60 min, pH 11.0, 2) methylene chloride, reflux, 2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Gellerstedt, Goeran; Hardell, Hanne-Lise; Lindfors, Eva-Lisa
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1980 , vol. 34, # 9 p. 669 - 674
反应条件
tert-butylamine in dimethyl sulfoxide T=40°C; 96 h;
参考文献
Lee Younghee; Sayre
Journal of the American Chemical Society, 1995 , vol. 117, # 48 p. 11823 - 11828
反应条件
dipotassium hydrogenphosphate; Fremy’s salt in water
0.0333333 h;
参考文献
Mure, Minae; Klinman, Judith P.
Journal of the American Chemical Society, 1995 , vol. 117, # 34 p. 8698 - 8706
反应条件
sodium hydroxide; dipotassium hydrogenphosphate; Fremy’s salt in methanol
T=0°C; 2 h;
参考文献
Mure, Minae; Klinman, Judith P.
Journal of the American Chemical Society, 1995 , vol. 117, # 34 p. 8698 - 8706
反应条件
1: 9.5 percent / 100percent H3PO4 / 45 °C
2: 91 percent / K2HPO4*3H2O, <(KSO3)2NO> / H2O / 0.03 h
View Scheme
参考文献
Mure, Minae; Klinman, Judith P.
Journal of the American Chemical Society, 1995 , vol. 117, # 34 p. 8698 - 8706
反应条件
sodium hydroxide; oxygen; Cu(II) perchlorate in water; acetonitrile
T=25°C; pH=10; 1.5 h;
参考文献
Ling, Ke-Qing; Lee, Younghee; Macikenas, Dainius; Protasiewicz, John D.; Sayre, Lawrence M.
Journal of Organic Chemistry, 2003 , vol. 68, # 4 p. 1358 - 1366
