1,3-苯并间二氧杂环戊烯-5-羧酰胺合成路线 （共 22 条）
反应条件
1: potassium carbonate 2: hydrogen chloride; ethanol; ethanolic solution 3: POCl3 View Scheme
参考文献
Vinkler; Szabo
Acta Chimica Academiae Scientiarum Hungaricae, 1955 , vol. 6, p. 323,330
反应条件
1: phosphorus (V)-chloride 2: ethanol; sodium carbonate; water; hydroxylamine hydrochloride View Scheme
参考文献
Andrewes; King; Walker
Proceedings of the Royal Society of London, Series B: Biological Sciences, 1946 , vol. 133, p. 20,30
反应条件
samarium diiodide; phosphoric acid in tetrahydrofuran 0.000833333 h; Ambient temperature;
参考文献
Kamochi; Kudo
Tetrahedron, 1992 , vol. 48, # 21 p. 4301 - 4312
反应条件
sodium hydroxide; alkaline aqueous sodium hypochlorite solution
参考文献
van Linge
Recueil des Travaux Chimiques des Pays-Bas, 1897 , vol. 16, p. 45
Full Text Show Details
Rupe; v. Majewski
Chemische Berichte, 1900 , vol. 33, p. 3405
反应条件
trifluoromethylsulfonic anhydride; triethylamine in dichloromethane 0.333333 h; Ambient temperature;
参考文献
Synthesis, , # 1 p. 64 - 65
反应条件
silver tetrafluoroborate; {1,3-bis[2,6-di(propan-2-yl)phenyl]-1,3-dihydro-2H-imidazol-2-ylidene}AuCl
T=100°C; Beckmann rearrangement; 20 h; Sealed tubeNeat (no solvent);
参考文献
Ramon, Ruben S.; Bosson, Johann; Diez-Gonzalez, Silvia; Marion, Nicolas; Nolan, Steven P.
Journal of Organic Chemistry, 2010 , vol. 75, # 4 p. 1197 - 1202
反应条件
CuSO4‵5H2O; hydroxylamine hydrochloride; sodium acetate
T=110°C; 2 h; Neat (no solvent);
参考文献
Ganguly, Nemai C.; Roy, Sushmita; Mondal, Pallab
Tetrahedron Letters, 2012 , vol. 53, # 11 p. 1413 - 1416
反应条件
water; [PtH(PMe2OH)((PMe2O...H...OPMe2)] in ethanol
T=80°C; 3.5 h;
参考文献
Jiang, Xiao-Bin; Minnaard, Adriaan J.; Feringa, Ben L.; De Vries, Johannes G.
Journal of Organic Chemistry, 2004 , vol. 69, # 7 p. 2327 - 2331
反应条件
ammonia; iodine in water
T=60°C; Lieben-Haller-Bauer reaction; 1 h;
参考文献
Cao, Liping; Ding, Jiaoyang; Gao, Meng; Wang, Zihua; Li, Juan; Wu, Anxin
Organic Letters, 2009 , vol. 11, # 17 p. 3810 - 3813
反应条件
1: With NbCl5 in 1,4-dioxane
2: With ammonia in 1,4-dioxane
T=45 - 50°C; 2 h;
参考文献
Nery, Marcelo S.; Ribeiro, Renata P.; Lopes, Claudio C.; Lopes, Rosangela S. C.
Synthesis, 2003 , # 2 p. 272 - 276
