噻吩并[3,4-b][1,4]苯并二恶英合成路线 （共 4 条）
反应条件
quinoline; copper chhromide in N,N-dimethyl acetamide
T=160°C; 0.5 h;
参考文献
Storsberg, Joachim; Schollmeyer, Dieter; Ritter, Helmut
Chemistry Letters, 2003 , vol. 32, # 2 p. 140 - 141
反应条件
1: 40 percent / K2CO3 / hexamethylphosphoric acid triamide / 3 h / 120 °C
2: NaOH; H2O / ethane-1,2-diol / 1 h / 110 °C
3: copper chhromide; quinoline / N,N-dimethyl-acetamide / 0.5 h / 160 °C
View Scheme
参考文献
Storsberg, Joachim; Schollmeyer, Dieter; Ritter, Helmut
Chemistry Letters, 2003 , vol. 32, # 2 p. 140 - 141
反应条件
1: NaOH; H2O / ethane-1,2-diol / 1 h / 110 °C
2: copper chhromide; quinoline / N,N-dimethyl-acetamide / 0.5 h / 160 °C
View Scheme
参考文献
Storsberg, Joachim; Schollmeyer, Dieter; Ritter, Helmut
Chemistry Letters, 2003 , vol. 32, # 2 p. 140 - 141
反应条件
toluene-4-sulfonic acid
T=90°C; Mitsunobu reaction;
参考文献
Poverenov, Elena; Sheynin, Yana; Zamoshchik, Natalia; Patra, Asit; Leitus, Gregory; Perepichka, Igor F.; Bendikov, Michael
Journal of Materials Chemistry, 2012 , vol. 22, # 29 p. 14645 - 14655
