2,4,5－三苯基咪唑合成路线 （共 149 条）
反应条件
1.1: CH2Cl2 / 1.5 h / -50 °C 1.2: 47 percent / CH2Cl2 / 4 h / -78 - 20 °C 2.1: 42 percent / tBuOK; nBuLi / tetrahydrofuran; hexane / 3 h / -40 °C View Scheme
参考文献
Habersaat, Nils; Froehlich, Roland; Wuerthwein, Ernst-Ulrich
European Journal of Organic Chemistry, 2004 , # 12 p. 2567 - 2581
反应条件
1: 76 percent / Zn / acetic acid / 1 h / Heating 2: 65 percent / Zn / acetic acid / 4 h / Heating View Scheme
参考文献
Nagy, Jozsef; Rapp, Rudolf; Alexovics, Maria; Doepp, Dietrich; Nyitrai, Jozsef; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 6 p. 661 - 666
反应条件
sodium T=190 - 200°C;
参考文献
Brunner
Justus Liebigs Annalen der Chemie, 1869 , vol. 151, p. 133
反应条件
ammonium acetate; acetic acid
参考文献
Bal'on, Ya. G.; Smirnov, V. A.
Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 9.2 p. 1712 - 1715
Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 9 p. 1983 - 1987
反应条件
ammonia T=100°C; im Rohr;
参考文献
Erdmann
Justus Liebigs Annalen der Chemie, 1865 , vol. 135, p. 182
Full Text Show Details
Laurent
Journal fuer Praktische Chemie (Leipzig), 1845 , vol. <1> 36, p. 5
Berzelius' Jahresber., vol. 26, p. 667
Full Text Show Details
Japp; Wilson
Journal of the Chemical Society, 1886 , vol. 49, p. 825,831
反应条件
1: NH2NH2 / ethanol / 4 h / Heating 2: NaNO2, AcOH / H2O 3: 96 percent / Heating 4: 10percent H2SO4 / ethanol / 20 h / Heating View Scheme
参考文献
Giammanco, Lorenzo; Invidiata, Francesco Paolo
Heterocycles, 1985 , vol. 23, # 6 p. 1459 - 1464
反应条件
in chloroform Rate constant;
参考文献
Borderie; Lavabre; Levy; Micheau; Laplante
Journal of the American Chemical Society, 1990 , vol. 112, # 11 p. 4105 - 4109
参考文献
Bakibaev, A.A.; Yagovkin, A.Yu.; Filimonov, V.D.
Journal of Organic Chemistry USSR (English Translation), 1991 , vol. 27, # 7 p. 1326 - 1331
Zhurnal Organicheskoi Khimii, 1991 , vol. 27, # 7 p. 1512 - 1519
反应条件
sulfuric acid in ethanol 20 h; Heating;
参考文献
Giammanco, Lorenzo; Invidiata, Francesco Paolo
Heterocycles, 1985 , vol. 23, # 6 p. 1459 - 1464
反应条件
1: NaNO2, AcOH / H2O 2: 96 percent / Heating 3: 10percent H2SO4 / ethanol / 20 h / Heating View Scheme
参考文献
Giammanco, Lorenzo; Invidiata, Francesco Paolo
Heterocycles, 1985 , vol. 23, # 6 p. 1459 - 1464
