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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
佛手柑内酯
合成路线
（共 25 条）
122850-55-9
→
反应条件
484-20-8
佛手柑内酯
反应条件
formic acid; triethylamine; palladium diacetate in N,N-dimethyl-formamide T=80°C; 11 h;
参考文献
Oda, Kazuaki; Nishizono, Naozumi; Tamai, Yukio; Yamaguchi, Yuki; Yoshimura, Teruki; Wada, Keiji; Machida, Minoru
Heterocycles, 2005 , vol. 65, # 8 p. 1985 - 1988
482-44-0
欧前胡素
→
反应条件
31575-93-6
白芷属脑
+
484-20-8
佛手柑内酯
+
1428263-43-7
+
1428263-44-8
+
1428263-45-9
+
1428263-47-1
+
1428417-34-8
+
1428263-46-0
+
1428417-33-7
反应条件
Penicillium janthinellum AS; liquid potato medium in acetone T=27°C; 120 h; Microbiological reaction;
参考文献
Lv, Xia; Liu, Dan; Hou, Jie; Dong, Peipei; Zhan, Libin; Wang, Li; Deng, Sa; Wang, Changyuan; Yao, Jihou; Shu, Xiaohong; Liu, Kexin; Ma, Xiaochi
Food Chemistry, 2013 , vol. 138, # 4 p. 2260 - 2266
108-73-6
间苯三酚
→
反应条件
484-20-8
佛手柑内酯
反应条件
1: 89 percent / dioxane / 12 h / 70 °C 2: 68 percent / ZnCl2 / 1.5 h / 90 °C 3: 82 percent / aq. NH4OH; iodine; aq. KI / dioxane / 0.83 h / ice cooling 4: 86 percent / K2CO3 / dimethylformamide / 0.25 h / 80 °C 5: 92 percent / OsO4; 2-methyl-2-propanol; NaIO4 / dioxane; H2O / 2 h / 20 °C 6: 71 percent / tetra-n-butylammonium bromide; BF3-Et2O / CHCl3 / 0.5 h / Heating 7: 90 percent / Et3N; formic acid / Pd(AcO)2 / dimethylformamide / 11 h / 80 °C View Scheme
参考文献
Oda, Kazuaki; Nishizono, Naozumi; Tamai, Yukio; Yamaguchi, Yuki; Yoshimura, Teruki; Wada, Keiji; Machida, Minoru
Heterocycles, 2005 , vol. 65, # 8 p. 1985 - 1988
2174-64-3
夫拉美诺
→
反应条件
484-20-8
佛手柑内酯
反应条件
1: 68 percent / ZnCl2 / 1.5 h / 90 °C 2: 82 percent / aq. NH4OH; iodine; aq. KI / dioxane / 0.83 h / ice cooling 3: 86 percent / K2CO3 / dimethylformamide / 0.25 h / 80 °C 4: 92 percent / OsO4; 2-methyl-2-propanol; NaIO4 / dioxane; H2O / 2 h / 20 °C 5: 71 percent / tetra-n-butylammonium bromide; BF3-Et2O / CHCl3 / 0.5 h / Heating 6: 90 percent / Et3N; formic acid / Pd(AcO)2 / dimethylformamide / 11 h / 80 °C View Scheme
参考文献
Oda, Kazuaki; Nishizono, Naozumi; Tamai, Yukio; Yamaguchi, Yuki; Yoshimura, Teruki; Wada, Keiji; Machida, Minoru
Heterocycles, 2005 , vol. 65, # 8 p. 1985 - 1988
3067-10-5
→
反应条件
484-20-8
佛手柑内酯
反应条件
1: 82 percent / aq. NH4OH; iodine; aq. KI / dioxane / 0.83 h / ice cooling 2: 86 percent / K2CO3 / dimethylformamide / 0.25 h / 80 °C 3: 92 percent / OsO4; 2-methyl-2-propanol; NaIO4 / dioxane; H2O / 2 h / 20 °C 4: 71 percent / tetra-n-butylammonium bromide; BF3-Et2O / CHCl3 / 0.5 h / Heating 5: 90 percent / Et3N; formic acid / Pd(AcO)2 / dimethylformamide / 11 h / 80 °C View Scheme
参考文献
Oda, Kazuaki; Nishizono, Naozumi; Tamai, Yukio; Yamaguchi, Yuki; Yoshimura, Teruki; Wada, Keiji; Machida, Minoru
Heterocycles, 2005 , vol. 65, # 8 p. 1985 - 1988
74794-29-9
→
反应条件
484-20-8
佛手柑内酯
反应条件
1: 86 percent / K2CO3 / dimethylformamide / 0.25 h / 80 °C 2: 92 percent / OsO4; 2-methyl-2-propanol; NaIO4 / dioxane; H2O / 2 h / 20 °C 3: 71 percent / tetra-n-butylammonium bromide; BF3-Et2O / CHCl3 / 0.5 h / Heating 4: 90 percent / Et3N; formic acid / Pd(AcO)2 / dimethylformamide / 11 h / 80 °C View Scheme
参考文献
Oda, Kazuaki; Nishizono, Naozumi; Tamai, Yukio; Yamaguchi, Yuki; Yoshimura, Teruki; Wada, Keiji; Machida, Minoru
Heterocycles, 2005 , vol. 65, # 8 p. 1985 - 1988
78045-69-9
→
反应条件
484-20-8
佛手柑内酯
反应条件
1: 92 percent / OsO4; 2-methyl-2-propanol; NaIO4 / dioxane; H2O / 2 h / 20 °C 2: 71 percent / tetra-n-butylammonium bromide; BF3-Et2O / CHCl3 / 0.5 h / Heating 3: 90 percent / Et3N; formic acid / Pd(AcO)2 / dimethylformamide / 11 h / 80 °C View Scheme
参考文献
Oda, Kazuaki; Nishizono, Naozumi; Tamai, Yukio; Yamaguchi, Yuki; Yoshimura, Teruki; Wada, Keiji; Machida, Minoru
Heterocycles, 2005 , vol. 65, # 8 p. 1985 - 1988
866081-74-5
→
反应条件
484-20-8
佛手柑内酯
反应条件
1: 71 percent / tetra-n-butylammonium bromide; BF3-Et2O / CHCl3 / 0.5 h / Heating 2: 90 percent / Et3N; formic acid / Pd(AcO)2 / dimethylformamide / 11 h / 80 °C View Scheme
参考文献
Oda, Kazuaki; Nishizono, Naozumi; Tamai, Yukio; Yamaguchi, Yuki; Yoshimura, Teruki; Wada, Keiji; Machida, Minoru
Heterocycles, 2005 , vol. 65, # 8 p. 1985 - 1988
866081-73-4
→
反应条件
484-20-8
佛手柑内酯
反应条件
1: 80 percent / NaIO4 / tetrahydrofuran; H2O / 72 h / 20 °C 2: 71 percent / tetra-n-butylammonium bromide; BF3-Et2O / CHCl3 / 0.5 h / Heating 3: 90 percent / Et3N; formic acid / Pd(AcO)2 / dimethylformamide / 11 h / 80 °C View Scheme
参考文献
Oda, Kazuaki; Nishizono, Naozumi; Tamai, Yukio; Yamaguchi, Yuki; Yoshimura, Teruki; Wada, Keiji; Machida, Minoru
Heterocycles, 2005 , vol. 65, # 8 p. 1985 - 1988
486-60-2
香柑醇
+
77-78-1
硫酸二甲酯
→
反应条件
484-20-8
佛手柑内酯
反应条件
potassium carbonate; acetone
参考文献
Stanley; Vannier
Journal of the American Chemical Society, 1957 , vol. 79, p. 3488,3490
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