2-甲基-3-硝基苯甲醚合成路线 （共 34 条）
反应条件
1: NBS, (PhCO)2O2 / CCl4 / Irradiation 2: aq. ethanol View Scheme
参考文献
Beckett,A.H. et al.
Tetrahedron, 1968 , vol. 24, p. 6093 - 6109
反应条件
potassium permanganate in water 4 h; Heating / reflux;
参考文献
Boehringer Ingelheim (Canada) Ltd.
Patent: US2004/106791 A1, 2004 ;
Location in patent: Page 15 ;
反应条件
1: potassium permanganate; water 2: iron (II)-hydroxide; aqueous ammonia View Scheme
参考文献
Roberts; Wiles; Kent
Journal of the Chemical Society, 1932 , p. 1792,1795
反应条件
1: N,N-dimethyl-formamide / 3 h / |Reflux 2: zinc; acetic acid; hydrogenchloride / water / 0.5 h / 20 °C 3: 4-(N,N-dimethlyamino)pyridine / acetonitrile / 20 °C 4: lithium diisopropyl amide / tetrahydrofuran / 1 h / 0 - 20 °C View Scheme
参考文献
SANOFI; ARNAUD, Joëlle; ARTIAGA, Martine; BARTH, Francis; HORTALA, Laurent; MARTINEZ, Serge; ROUX, Pascale
Patent: WO2013/87643 A1, 2013 ;
反应条件
1: EtOK / ethanol / Heating 2: aq. HCl 3: FeSO4/NH3 View Scheme
参考文献
Blaikie; Perkin
Journal of the Chemical Society, 1924 , vol. 125, p. 313
反应条件
1: tin; aqueous hydrochloric acid 2: aqueous H2SO4 / Diazotization 4: aluminium chloride; carbon disulfide 5: fuming sulfuric acid 6: AlCl3 / 200 °C / durch langsames Erhitzen View Scheme
参考文献
Mitter; Biswas
Journal of the Indian Chemical Society, 1930 , vol. 7, p. 839
反应条件
hydrogen; palladium on activated carbon in ethanol T=20°C; 3 h;
参考文献
Seike, Hisayuki; Matsugi, Takeshi; Shimazaki, Atsushi
Patent: US2009/12123 A1, 2009 ;
Location in patent: Page/Page column 14-15 ;
反应条件
1: EtOK / ethanol / Heating 2: aq. HCl 3: FeSO4/NH3 View Scheme
参考文献
Fagan, Gay P.; Chapleo, Christopher B.; Lane, Anthony C.; Myers, Malcolm; Roach, Alan G.; et al
Journal of Medicinal Chemistry, 1988 , vol. 31, # 5 p. 944 - 948
反应条件
1: tin; aqueous hydrochloric acid 2: aqueous H2SO4 / Diazotization View Scheme
参考文献
Mitter; Biswas
Journal of the Indian Chemical Society, 1930 , vol. 7, p. 839
反应条件
carbon disulfide; chromium oxychloride
参考文献
Wani,M.C.; Wall,M.E.
Journal of Organic Chemistry, 1969 , vol. 34, # 5 p. 1364 - 1367
