N-苯甲酰-2'-脱氧胞苷合成路线 (共 36 条)
反应条件
in methanol 10 h; Heating;
参考文献
Charubala, R.; Uhlmann, E.; Beiter, A. H.; Pfleiderer, W.
Synthesis, 1984 , # 11 p. 965 - 968
反应条件
pyridine; chloro-trimethyl-silane
参考文献
Lucas; Elchinger; Faugeras; Zerrouki
Nucleosides, Nucleotides and Nucleic Acids, 2010 , vol. 29, # 3 p. 168 - 177
反应条件
phosphate buffer; Candida antarctica Lipase A in 1,4-dioxane T=40°C; pH=7; 96 h;
参考文献
Garcia, Javier; Fernandez, Susana; Ferrero, Miguel; Sanghvi, Yogesh S.; Gotor, Vicente
Journal of Organic Chemistry, 2002 , vol. 67, # 13 p. 4513 - 4519
反应条件
1: H2O; pyridine / 0.5 h / 20 °C 2: pyridine / 4 h / 20 °C 3: aq. NH4OH / 0.25 h / 20 °C View Scheme
参考文献
Busson; Kerremans; Van Aerschot; Peeters; Blaton; Herdewijn
Nucleosides and Nucleotides, 1999 , vol. 18, # 4-5 p. 1079 - 1082
反应条件
sodium hydroxide in pyridine; methanol 0.00333333 h; microwave irradiation;
参考文献
Rao; Kumar; Chauhan; Garg; Gupta
Nucleosides, Nucleotides and Nucleic Acids, 2002 , vol. 21, # 4-5 p. 393 - 400
反应条件
in pyridine T=80°C; 5 h;
参考文献
Igolen, Jean; Morin, Christophe
Journal of Organic Chemistry, 1980 , vol. 45, # 23 p. 4802 - 4804
反应条件
1: benzoic acid With 4-methyl-morpholine; 2-chloro-4,6-dimethoxy-[1,3,5]triazine in dichloromethane T=20°C; 2: [14C]-Deoxycytidine in dichloromethane; N,N-dimethyl-formamide T=20 - 50°C;
参考文献
Rode, Ambadas B.; Son, Sang Jun; Hong, In Seok
Bulletin of the Korean Chemical Society, 2010 , vol. 31, # 7 p. 2061 - 2064
反应条件
1: pyridine / 4 h / 20 °C 2: aq. NH4OH / 0.25 h / 20 °C View Scheme
参考文献
Ti, G. S.; Gaffney, B. L.; Jones, R. A.
Journal of the American Chemical Society, 1982 , vol. 104, # 5 p. 1316 - 1319
反应条件
trichloroacetic acid in dichloromethane 0.00833333 h; Ambient temperaturesynthesis is carried out on a silica support;
参考文献
Rejman, Dominik; Kralikova, Sarka; Tocik, Zdenek; Liboska, Radek; Rosenberg, Ivan
Collection of Czechoslovak Chemical Communications, 2002 , vol. 67, # 4 p. 502 - 508
反应条件
1: pyridine / 2 h / Ambient temperature 2: 29percent aq. ammonia / pyridine / 0.25 h / Ambient temperature View Scheme
参考文献
Busson; Kerremans; Van Aerschot; Peeters; Blaton; Herdewijn
Nucleosides and Nucleotides, 1999 , vol. 18, # 4-5 p. 1079 - 1082