2-羟基-3-甲基-1,4-萘醌合成路线 （共 82 条）
反应条件
air; phthalocyanine[Fe(3+)]; Montmorillonite K10 in methanol
T=20°C; 1 h;
参考文献
Villemin, Didier; Hammadi, Mohamed; Hachemi, Messaoud
Synthetic Communications, 2002 , vol. 32, # 10 p. 1501 - 1515
反应条件
sodium hydroxide; water
参考文献
Baker et al.
Journal of the American Chemical Society, 1942 , vol. 64, p. 1096,1100
反应条件
1: NaH / tetrahydrofuran / 0.5 h / Ambient temperature
2: 92 percent / tetrahydrofuran / 0.5 h / Ambient temperature
3: 94 percent / 2,6-lutidine, LiI*2H2O / 1 h / 150 °C
4: 72 percent / m-chloroberbenzoic acid / CH2Cl2 / 1 h / Ambient temperature
5: 1.) aq. Na2S2O4, 2.) t-BuOK, O2 / 1.) benzene, 2 min, 2.) t-BuOH, 5 min.
View Scheme
参考文献
Ghera, Eugene; Ben-David, Yoshua
Journal of Organic Chemistry, 1985 , vol. 50, # 18 p. 3355 - 3359
反应条件
1: 94 percent / 2,6-lutidine, LiI*2H2O / 1 h / 150 °C
2: 72 percent / m-chloroberbenzoic acid / CH2Cl2 / 1 h / Ambient temperature
3: 1.) aq. Na2S2O4, 2.) t-BuOK, O2 / 1.) benzene, 2 min, 2.) t-BuOH, 5 min.
View Scheme
参考文献
Ghera, Eugene; Ben-David, Yoshua
Journal of Organic Chemistry, 1985 , vol. 50, # 18 p. 3355 - 3359
反应条件
1: 1.) t-BuLi / 1.) tetrahydropyran, pentane, 4 h, 2.) -40 deg C, 4h
2: Fremy's salt / methanol; H2O / 0.5 h
View Scheme
参考文献
Coll, Gloria; Morey, Jeroni; Costa, Antoni; Saa,Jose M.
Journal of Organic Chemistry, 1988 , vol. 53, # 22 p. 5345 - 5348
参考文献
Tarbell et al.
Journal of the American Chemical Society, 1950 , vol. 72, p. 379,381
反应条件
selenium(IV) oxide; dihydrogen peroxide in tetrahydrofuran
48 h; Heating;
参考文献
Brzaszcz; Kloc; Maposah; Mlochowski
Synthetic Communications, 2000 , vol. 30, # 24 p. 4425 - 4434
反应条件
in benzene
Ambient temperatureIrradiation;
参考文献
Maruyama, Kazuhiro; Osuka, Atsuhiro; Suzuki, Hitomi
Journal of the Chemical Society, Chemical Communications, 1980 , # 7 p. 323 - 324
反应条件
in tert-butyl alcohol; benzene
3 h; Irradiation;
参考文献
Osuka, Atsuhiro
Journal of Organic Chemistry, 1982 , vol. 47, # 16 p. 3131 - 3139
反应条件
hydrogenchloride in diethyl ether
参考文献
Eistert,B.; Ganster,O.
Chemische Berichte, 1971 , vol. 104, p. 78 - 86
