2,3-二甲氧基-5,6-二甲基对苯醌合成路线 （共 21 条）
反应条件
(NH4)2S2O8; silver nitrate in water; acetonitrile
T=65°C; 3.5 h;
参考文献
Ma, Wei; Zhou, Hao; Ying, Yi-Lun; Li, Da-Wei; Chen, Guo-Rong; Long, Yi-Tao; Chen, Hong-Yuan
Tetrahedron, 2011 , vol. 67, # 33 p. 5990 - 6000
反应条件
hydrogenchloride; iron(III) chloride
参考文献
Vischer
Journal of the Chemical Society, 1953 , p. 815,818
反应条件
1: Al(OiPr)3 / propan-2-ol
2: (i) H2, aq. HCl, Pd-C, (ii) aq. FeCl3
3: K2CO3 / acetone
4: aq. Na2S2O3 / diethyl ether
6: aq. FeCl3 / diethyl ether
View Scheme
参考文献
Koshi,K.; Shimizu,M.
Chemical and Pharmaceutical Bulletin, 1968 , vol. 16, p. 2343 - 2350
反应条件
1: NO2/HNO3 / acetic acid
2: Al(OiPr)3 / propan-2-ol
3: (i) H2, aq. HCl, Pd-C, (ii) aq. FeCl3
4: K2CO3 / acetone
5: aq. Na2S2O3 / diethyl ether
7: aq. FeCl3 / diethyl ether
View Scheme
参考文献
Koshi,K.; Shimizu,M.
Chemical and Pharmaceutical Bulletin, 1968 , vol. 16, p. 2343 - 2350
反应条件
1: K2CO3, KI / acetone
2: aq. H2SO4 / acetic acid
3: (i) H2, aq. HCl, Pd-C, (ii) aq. FeCl3
4: K2CO3 / acetone
5: aq. Na2S2O3 / diethyl ether
7: aq. FeCl3 / diethyl ether
View Scheme
参考文献
Koshi,K.; Shimizu,M.
Chemical and Pharmaceutical Bulletin, 1968 , vol. 16, p. 2343 - 2350
反应条件
1: aq. Na2S2O3 / diethyl ether
3: aq. FeCl3 / diethyl ether
View Scheme
参考文献
Koshi,K.; Shimizu,M.
Chemical and Pharmaceutical Bulletin, 1968 , vol. 16, p. 2343 - 2350
反应条件
1: (i) H2, aq. HCl, Pd-C, (ii) FeCl3, aq. HCl
2: aq. Na2S2O3 / diethyl ether
4: aq. FeCl3 / diethyl ether
View Scheme
参考文献
Koshi,K.; Shimizu,M.
Chemical and Pharmaceutical Bulletin, 1968 , vol. 16, p. 2343 - 2350
反应条件
1: Al(OiPr)3 / propan-2-ol
2: (i) H2, aq. HCl, Pd-C, (ii) FeCl3, aq. HCl
3: aq. Na2S2O3 / diethyl ether
5: aq. FeCl3 / diethyl ether
View Scheme
参考文献
Koshi,K.; Shimizu,M.
Chemical and Pharmaceutical Bulletin, 1968 , vol. 16, p. 2343 - 2350
反应条件
1: K2CO3 / acetone
2: aq. Na2S2O3 / diethyl ether
4: aq. FeCl3 / diethyl ether
View Scheme
参考文献
Koshi,K.; Shimizu,M.
Chemical and Pharmaceutical Bulletin, 1968 , vol. 16, p. 2343 - 2350
反应条件
1: (i) H2, aq. HCl, Pd-C, (ii) aq. FeCl3
2: K2CO3 / acetone
3: aq. Na2S2O3 / diethyl ether
5: aq. FeCl3 / diethyl ether
View Scheme
参考文献
Koshi,K.; Shimizu,M.
Chemical and Pharmaceutical Bulletin, 1968 , vol. 16, p. 2343 - 2350
