1: With (Ph)2SiH2; bis(1,5-cyclooctadiene)-rhodium(I) tetrafluoroborate; (S,S)-2,2''-bis{(R)-1-(di-n-butylphosphino)ethyl}-1,1''-biferrocene in tetrahydrofuran T=-40°C; hydrosilylation; 3 h; 2: With methanol; potassium carbonate in tetrahydrofuran T=20°C; methanolysis; 4 h; Title compound not separated from byproducts;
参考文献
Kuwano, Ryoichi; Sawamura, Masaya; Shirai, Junya; Takahashi, Masatoshi; Ito, Yoshihiko
Bulletin of the Chemical Society of Japan, 2000 , vol. 73, # 2 p. 485 - 496
