反应条件
1: 68 percent / NaH / hexamethylphosphoric acid triamide; tetrahydrofuran / 1.) 0 deg C, 2.) 23 deg C
2: 87 percent / n-Bu4NF*3H2O / dimethylformamide / 55 °C
3: 35 percent / PDC / CH2Cl2 / 23 °C
4: 1.) ceric ammonium nitrate, 2.) 1 N HCl / 1.) CH3CN, H2O, 0 deg C, 2.) H2O, MeOH, 23 deg C
View Scheme
参考文献
Yamashita, Ayako
Journal of the American Chemical Society, 1985 , vol. 107, # 20 p. 5823 - 5824
