2,6-二甲基-4-硝基吡啶 1-氧化物合成路线 （共 14 条）
反应条件
1: 86 percent / aq. HCl / 200 °C 2: 100 percent / PCl3 / CHCl3 View Scheme
参考文献
Yoakim; Bonneau; Deziel; Doyon; Duan; Guse; Landry; Malenfant; Naud; Ogilvie; O'Meara; Plante; Simoneau; Thavonekham; Boes; Cordingley
Bioorganic and Medicinal Chemistry Letters, 2004 , vol. 14, # 3 p. 739 - 742
反应条件
hydrogen; acetic acid; palladium on activated charcoal T=50°C; P=2327.2 Torr; 19 h;
参考文献
Tanga; Bupp; Tochimoto
Journal of Heterocyclic Chemistry, 1997 , vol. 34, # 3 p. 717 - 727
反应条件
1: methanol 2: platinum /palladium/charcoal; acetic acid anhydride / Hydrogenation View Scheme
参考文献
Zohuri, Gholam Hossein; Seyedi, Seyed Mohammad; Sandaroos, Reza; Damavandi, Saman; Mohammadi, Ali
Catalysis Letters, 2010 , vol. 140, # 3-4 p. 160 - 166
反应条件
palladium on activated charcoal; water
参考文献
Kato; Hamaguchi
Pharmaceutical Bulletin, 1956 , vol. 4, p. 174,177
反应条件
Bi(NO3)3; sulfuric acid; silica gel
T=25°C; 0.166667 h;
参考文献
Chen, Hongfeng; Sweet, James A.; Lam, Kin-Chung; Rheingold, Arnold L.; McGrath, Dominic V.
Tetrahedron Asymmetry, 2009 , vol. 20, # 14 p. 1672 - 1682
反应条件
1: 85 percent / mCPBA / CH2Cl2
2: 59 percent / HNO3; H2SO4 / 80 °C
View Scheme
参考文献
Yoakim; Bonneau; Deziel; Doyon; Duan; Guse; Landry; Malenfant; Naud; Ogilvie; O'Meara; Plante; Simoneau; Thavonekham; Boes; Cordingley
Bioorganic and Medicinal Chemistry Letters, 2004 , vol. 14, # 3 p. 739 - 742
反应条件
ethyl mercaptan sodium salt in dimethyl sulfoxide
Ambient temperature;
参考文献
Ban-Oganowska, Hanna; Talik, Tadeusz
Polish Journal of Chemistry, 1980 , vol. 54, # 5 p. 1041 - 1048
反应条件
sulfuric acid; potassium nitrate
参考文献
Ochiai et al.
Yakugaku Zasshi, 1943 , vol. 63, p. 79,83
Chem.Abstr., 1951 , p. 5151
反应条件
triethylbutylammonium chloride; ethenetetracarbonitrile in acetonitrile
T=65°C; 5 h;
参考文献
Nizhnik; Andreev; Belashev
Russian Journal of Organic Chemistry, 2008 , vol. 44, # 12 p. 1824 - 1830
反应条件
1: 86 percent / aq. HCl / 200 °C
2: 100 percent / PCl3 / CHCl3
3: 52 percent / NaSH / dimethylformamide / 140 °C
View Scheme
参考文献
Yoakim; Bonneau; Deziel; Doyon; Duan; Guse; Landry; Malenfant; Naud; Ogilvie; O'Meara; Plante; Simoneau; Thavonekham; Boes; Cordingley
Bioorganic and Medicinal Chemistry Letters, 2004 , vol. 14, # 3 p. 739 - 742
