H-丝氨酰(TBU)-OTBU合成路线 （共 6 条）
反应条件
perchloric acid in water
4 h;
参考文献
Souto, Alba; Montaos, Marcos A.; Balado, Miguel; Osorio, Carlos R.; Rodriguez, Jaime; Lemos, Manuel L.; Jimenez, Carlos
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 1 p. 295 - 302
反应条件
hydrogen; palladium on activated charcoal in ethanol
参考文献
Callahan,F.M. et al.
Journal of the American Chemical Society, 1963 , vol. 85, p. 201 - 207
反应条件
sulfuric acid
T=25°C; 2 h; Molecular sieve; chemoselective reaction;
参考文献
Mallesha; Prahlada Rao; Suhas; Channe Gowda
Tetrahedron Letters, 2012 , vol. 53, # 6 p. 641 - 645
反应条件
sulfuric acid in 1,4-dioxane
参考文献
Schroeder,E.
Justus Liebigs Annalen der Chemie, 1963 , vol. 670, p. 127 - 136
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Reggelin, Michael; Junker, Bernd; Heinrich, Timo; Slavik, Stefan; Buehle, Philipp
Journal of the American Chemical Society, 2006 , vol. 128, # 12 p. 4023 - 4034
反应条件
tri-n-butyl-tin hydride; toluene-4-sulfonic acid; bis-triphenylphosphine-palladium(II) chloride
1.) moist dichloromethane, room temperature; Yield given. Multistep reaction;
参考文献
Guibe, F.; Dangles, O.; Balavoine, G.
Tetrahedron Letters, 1986 , vol. 27, # 21 p. 2365 - 2368
反应条件
(i) H2SO4, CH2Cl2, (ii) H2, Pd-BaSO4, MeOH; Multistep reaction;
参考文献
Beyerman,H.C.; Bontekoe,J.S.
Recueil des Travaux Chimiques des Pays-Bas, 1962 , vol. 81, p. 691 - 698
