5,5'-二溴-2,2'-联噻吩合成路线 （共 35 条）
反应条件
benzyltrimethylammonium bromide dibromide; zinc(II) chloride in acetic acid 27 h; Ambient temperature;
参考文献
Okamoto, Tsuyoshi; Kakinami, Takaaki; Fujimoto, Hiroshi; Kajigaeshi, Shoji
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 8 p. 2566 - 2568
反应条件
1: With n-butyllithium in diethyl ether T=-78°C; 2 h; 2: With copper(ll) bromide in diethyl ether T=-78 - 20°C;
参考文献
Wang, Nai-Xing
Synthetic Communications, 2003 , vol. 33, # 12 p. 2119 - 2124
反应条件
1: With potassium fluoride; silver nitrate; PdCl2(PPh)3 in dimethyl sulfoxide T=20°C; 12 h; 2: With potassium fluoride; silver nitrate in dimethyl sulfoxide 12 h;
参考文献
Takahashi, Masabumi; Masui, Kentaro; Sekiguchi, Hiroki; Kobayashi, Nobuhiko; Mori, Atsunori; Funahashi, Masahiro; Tamaoki, Nobuyuki
Journal of the American Chemical Society, 2006 , vol. 128, # 33 p. 10930 - 10933
反应条件
2-bromo-3,4-dichloropyridazin-3(2H)-one; zinc dibromide in dichloromethane T=20°C; 0.0833333 h; regioselective reaction;
参考文献
Nakayama, Juzo; Konishi, Toru; Murabayashi, Shigeru; Hoshino, Masamatsu
Heterocycles, 1987 , vol. 26, # 7 p. 1793 - 1796
反应条件
copper dichloride in diethyl ether T=-78°C; 2 h;
参考文献
Dahlmann, Uwe; Neidlein, Richard
Helvetica Chimica Acta, 1996 , vol. 79, # 3 p. 755 - 766
反应条件
2-bromo-3,4-dichloropyridazin-3(2H)-one; zinc dibromide in dichloromethane T=20°C; 0.0833333 h; regioselective reaction;
参考文献
Jung, Kwang-Ju; Seung, Beom Kang; Won, Ju-Eun; Park, Song-Eun; Ki, Hun Park; Jong, Keun Park; Lee, Sang-Gyeong; Yoon, Yong-Jin
Synlett, 2009 , # 3 p. 490 - 494
反应条件
palladium diacetate; silver(l) oxide; biphenyl-2-carboxylic acid in dimethyl sulfoxide T=80°C; 8 h;
参考文献
He, Chun-Yang; Wang, Zhen; Wu, Cai-Zhi; Qing, Feng-Ling; Zhang, Xingang
Chemical Science, 2013 , vol. 4, # 9 p. 3508 - 3513
反应条件
lead(IV) tetraacetate; lithium bromide; lithium iodide in chloroform T=20°C; 0.5 h; regioselective reaction;
参考文献
Kim, Bo Ram; Kim, Eun Jung; Sung, Gi Hyeon; Kim, Jeum-Jong; Shin, Dong-Soo; Lee, Sang-Gyeong; Yoon, Yong-Jin
European Journal of Organic Chemistry, 2013 , # 14 p. 2788 - 2791
反应条件
Au(OAc)3; (1S)-10-camphorsulfonic acid in chloroform-d1; methanol-d4 T=25°C; 2 h;
参考文献
Ball, Liam T.; Lloyd-Jones, Guy C.; Russell, Christopher A.
Journal of the American Chemical Society, 2014 , vol. 136, # 1 p. 254 - 264
反应条件
1: 2-bromo-5-(5-bromothiophen-2-yl)thiophene With n-butyllithium in tetrahydrofuran T=-78 - 20°C; 2: tri-isopropoxy-borane in tetrahydrofuran T=-78 - 20°C; 12 h;
参考文献
Henze, Oliver; Parker, David; Feast, W. James
Journal of Materials Chemistry, 2003 , vol. 13, # 6 p. 1269 - 1273
