(2,4-二氟苯基乙炔)三甲基硅烷合成路线 (共 2 条)
反应条件
zinc(II) chloride in 1,2-dichloro-ethane
T=150°C; 0.25 h; microwave irradiation;
参考文献
Yeager, Adam R.; Min, Geanna K.; Porco Jr., John A.; Schaus, Scott E.
Organic Letters, 2006 , vol. 8, # 22 p. 5065 - 5068
反应条件
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine
Sonogashira coupling; 24 h; Inert atmosphereReflux;
参考文献
Ladouceur, Sebastien; Soliman, Ahmed M.; Zysman-Colman, Eli
Synthesis, 2011 , # 22 art. no. M79111SS, p. 3604 - 3611