3-(1,3-二氧戊环)苯硼酸合成路线 （共 2 条）
反应条件
hydrogenchloride in ethyl acetate; acetone T=20°C; 1 h; Inert atmosphere;
参考文献
Molander, Gary A.; Trice, Sarah L. J.; Kennedy, Steven M.; Dreher, Spencer D.; Tudge, Matthew T.
Journal of the American Chemical Society, 2012 , vol. 134, # 28 p. 11667 - 11673
反应条件
1: With n-butyllithium in tetrahydrofuran
T=-78°C; 0.166667 h; Inert atmosphere;
2: With tri-isopropoxy-borane in tetrahydrofuran
T=-78 - 20°C; 1 h; Inert atmosphere;
3: With water; ammonium chloride in tetrahydrofuran
0.5 h;
参考文献
Bonin, Helene; Delbrayelle, Dominique; Demonchaux, Patrice; Gras, Emmanuel
Chemical Communications, 2010 , vol. 46, # 15 p. 2677 - 2679
