2,4-二羟基-6-甲基苯甲酸合成路线 （共 54 条）
反应条件
sodium chlorite; sodium dihydrogenphosphate in water; dimethyl sulfoxide
参考文献
UNIVERSITY OF IOWA RESEARCH FOUNDATION; JIN, Zhendong; KANG, Ying
Patent: WO2004/58738 A1, 2004 ;
Location in patent: Page 2/2; 10 ;
反应条件
Armillaria mellea iterative type I polyketide synthase ArmB, N-terminal hexahistidine-tagged protein in aq. phosphate buffer pH=7.4; 20 h; Enzymatic reaction;
参考文献
Lackner, Gerald; Bohnert, Markus; Wick, Jonas; Hoffmeister, Dirk
Chemistry and Biology, 2013 , vol. 20, # 9 p. 1101 - 1106
反应条件
1.1: POCl3 / 12 h / 20 °C 1.2: 80 percent / NaOH / H2O / 0.17 h / pH 10 / Heating 2.1: 77 percent / NaH2PO4; NaClO2 / H2O; dimethylsulfoxide / 20 °C View Scheme
参考文献
Kang, Ying; Mei, Yan; Du, Yuguo; Jin, Zhendong
Organic Letters, 2003 , vol. 5, # 23 p. 4481 - 4484
反应条件
aluminium trichloride in chlorobenzene 0.75 h; Heating;
参考文献
Evans, Geoffrey E.; Staunton, James
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 755 - 762
参考文献
Harris,T.M. et al.
Journal of the American Chemical Society, 1976 , vol. 98, p. 7733 - 7741
反应条件
sulfuric acid in water T=0°C; 0.166667 h;
参考文献
Rawat; Shukla, Vertika; Negi, Sandeep; Pant
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006 , vol. 45, # 11 p. 2566 - 2570
反应条件
calcium hydroxide powder
参考文献
Hesse
Journal fuer Praktische Chemie (Leipzig), 1898 , vol. <2> 57, p. 306,307
Journal fuer Praktische Chemie (Leipzig), 1900 , vol. 62, p. 342
参考文献
Fujii; Osumi
Yakugaku Zasshi, 1936 , vol. 56, p. 531,537; dtsch. Ref. S. 101
Chem.Abstr., 1936 , p. 8189
反应条件
sodium hydroxide T=20°C;
参考文献
Kato,T.; Hozumi,T.
Chemical and Pharmaceutical Bulletin, 1972 , vol. 20, p. 1574 - 1578
反应条件
1: 1.) butyl-lithium / 1.) ether, hexane, -78 deg C, 1 h; 2.) ether, hexane, up to RT 2: 54 percent / aluminum chloride / chlorobenzene / 0.75 h / Heating View Scheme
参考文献
Evans, Geoffrey E.; Staunton, James
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 755 - 762
