2-己烯-4-醇, CIS + TRANS合成路线 (共 34 条)
反应条件
lithium aluminium tetrahydride in water
参考文献
Schleyer; Niessen; Bargon
New Journal of Chemistry, 2001 , vol. 25, # 3 p. 423 - 426
反应条件
lithium borohydride; borane in tetrahydrofuran T=-50°C; 2 h;
参考文献
Arase, Akira; Hoshi, Masayuki; Yamaki, Tuneharu; Nakanishi, Hirohumi
Journal of the Chemical Society, Chemical Communications, 1994 , # 7 p. 855 - 856
反应条件
isopropyl alcohol; magnesium oxide T=250°C;
参考文献
Kaspar, J.; Trovarelli, A.; Lenarda, M.; Graziani, M.
Tetrahedron Letters, 1989 , vol. 30, # 20 p. 2705 - 2706
反应条件
lt;(P)-NMe2 = o-(diphenylphosphino)-N,N-dimethyl anilinegt;; H2Irlt;*gt;lt;(P)-NClt;*gt;H2Megt;lt;(P)-NMe2gt; in isopropyl alcohol T=83°C; 7 h;
参考文献
Farnetti, Erica; Nardin, Giorgio; Graziani, Mauro
Journal of the Chemical Society, Chemical Communications, 1989 , # 17 p. 1264 - 1265
参考文献
Kieffer,R.
Bulletin de la Societe Chimique de France, 1967 , p. 3026 - 3029
参考文献
Frankel, Edwin N.; Garwood, Robert F.; Vinson, John R.; Weedon, Basil C. L.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 11 p. 2707 - 2714
反应条件
1: With [2-(methoxymethy)phenyl]phenylsilane; RhCl(PPh3)3 T=20°C; 2: With hydrogenchloride
参考文献
Imao, Daisuke; Hayama, Miyuki; Ishikawa, Kohta; Ohta, Tetsuo; Ito, Yoshihiko
Chemistry Letters, 2007 , vol. 36, # 3 p. 366 - 367
反应条件
Amberlite IRA-400; borohydride form in methanol T=20°C; Reduction; 3 h;
参考文献
Sim, Tae Bo; Yoon, Nung Min
Bulletin of the Chemical Society of Japan, 1997 , vol. 70, # 5 p. 1101 - 1107
反应条件
magnesium 1.) ether, 2 h, reflux 2.) -30 deg C to room temp.; Yield given. Multistep reaction;
参考文献
Bouchoux, Guy; Hoppilliard, Yannik; Jaudon, Pascale
Organic Mass Spectrometry, 1987 , vol. 22, p. 98 - 102
参考文献
Delaby; Morel
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1925 , vol. 180, p. 1409
Bulletin de la Societe Chimique de France, 1926 , vol. <4>39, p. 226
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Prevost
Annales de Chimie (Cachan, France), 1928 , vol. <10>10, p. 178,179
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1926 , vol. 183, p. 744